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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
21849-91-2
合成路线
（共 17 条）
1246204-76-1
→
反应条件
21849-91-2
反应条件
1: With methyl trifluoromethanesulfonate in toluene T=100°C; 2 h; Inert atmosphere; 2: With methanol; sodium T=80°C; 0.25 h; Inert atmosphere;
参考文献
Ackermann, Lutz; Diers, Emelyne; Manvar, Atul
Organic Letters, 2012 , vol. 14, # 4 p. 1154 - 1157
533-58-4
2-碘苯酚
+
5720-07-0
4-甲氧基苯硼酸
→
反应条件
21849-91-2
反应条件
palladium 10 on activated carbon; potassium carbonate in water T=80°C; Suzuki-Miyaura Coupling; 2.5 h; Inert atmosphere;
参考文献
Schmidt, Bernd; Riemer, Martin
Journal of Organic Chemistry, 2014 , vol. 79, # 9 p. 4104 - 4118
95-56-7
邻溴苯酚
+
5720-07-0
4-甲氧基苯硼酸
→
反应条件
21849-91-2
反应条件
palladium diacetate; potassium carbonate in water T=80°C; Suzuki Coupling; 1.5 h; Sealed tube;
参考文献
Xiang, Liu; Xiaohua, Zhao; Ming, Lu
Applied Organometallic Chemistry, 2013 , vol. 27, # 10 p. 615 - 618
928642-45-9
+
696-62-8
4-碘苯甲醚
→
反应条件
21849-91-2
反应条件
potassium phosphate; tetrakis(triphenylphosphine) palladium(0) in 1,4-dioxane T=50°C; 32 h; Inert atmosphere;
参考文献
Yang, Ke; Zhang, Jun; Li, Yun; Cheng, Bin; Zhao, Liang; Zhai, Hongbin
Organic Letters, 2013 , vol. 15, # 4 p. 808 - 811
63828-70-6
→
反应条件
21849-91-2
反应条件
hydrogen bromide; oxygen; copper(ll) bromide in 1,4-dioxane; water T=20°C; 40 h; Sealed tube;
参考文献
Kikushima, Kotaro; Nishina, Yuta
RSC Advances, 2013 , vol. 3, # 43 p. 20150 - 20156
104-92-7
4-溴苯甲醚
+
89466-08-0
2-羟基苯硼酸
→
反应条件
21849-91-2
反应条件
palladium 10 on activated carbon; tetra-n-butylammonium fluoride trihydrate T=150°C; Suzuki-Miyaura Coupling; 0.5 h; Microwave irradiationInert atmosphere;
参考文献
Schmidt, Bernd; Riemer, Martin
Journal of Organic Chemistry, 2014 , vol. 79, # 9 p. 4104 - 4118
104-92-7
4-溴苯甲醚
→
反应条件
21849-91-2
反应条件
dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; potassium phosphate; palladium diacetate in 1,4-dioxane; water T=23 - 100°C; Suzuki Coupling; 12 h; Inert atmosphere;
参考文献
Ahn, Su-Jin; Lee, Chun-Young; Cheon, Cheol-Hong
Advanced Synthesis and Catalysis, 2014 , vol. 356, # 8 p. 1767 - 1772
95-57-8
邻氯苯酚
+
13139-86-1
3-甲基-CBS-氧硼啶
→
反应条件
21849-91-2
反应条件
1: 4-methoxyphenyl magnesium bromide With C24H52Cl2O12P4Pd2 in tetrahydrofuran; 1,4-dioxane T=20°C; Kumada-Corriu cross-coupling reaction; 0.0833333 h; Inert atmosphere; 2: 2-chlorophenol in tetrahydrofuran; 1,4-dioxane T=110°C; Kumada-Corriu cross-coupling reaction; 24 h; Inert atmosphere; chemoselective reaction;
参考文献
Ackermann, Lutz; Kapdi, Anant R.; Fenner, Sabine; Kornhaab, Christoph; Schulzke, Carola
Chemistry - A European Journal, 2011 , vol. 17, # 10 p. 2965 - 2971
65109-75-3
+
100-66-3
苯甲醚
→
反应条件
21849-91-2
+
3594-88-5
+
16881-71-3
4-羟基-4-甲氧基联二苯
+
65109-82-2
反应条件
trifluorormethanesulfonic acid; trifluoroacetic acid T=0°C; 1 h;
参考文献
Endo, Yasuyuki; Shudo, Koichi; Okamoto, Toshihiko
Journal of the American Chemical Society, 1982 , vol. 104, # 23 p. 6393 - 6397
696-62-8
4-碘苯甲醚
+
89466-08-0
2-羟基苯硼酸
→
反应条件
21849-91-2
反应条件
potassium fluoride; palladium 10 on activated carbon; potassium carbonate in water T=80°C; Suzuki-Miyaura Coupling; 2.5 h; Inert atmosphere;
参考文献
Schmidt, Bernd; Riemer, Martin
Journal of Organic Chemistry, 2014 , vol. 79, # 9 p. 4104 - 4118
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