2-对甲苯氧基甲基环氧乙烷合成路线 （共 23 条）
反应条件
in hexane T=20°C; 2 h; Irradiation; Quantum yield;
参考文献
Timpe, H.-J.; Garcia, C.; Fedtke, M.
Journal fuer Praktische Chemie (Leipzig), 1985 , vol. 327, # 4 p. 616 - 626
反应条件
T=20°C; 2 h; Irradiation; Quantum yield;
参考文献
Timpe, H.-J.; Garcia, C.; Fedtke, M.
Journal fuer Praktische Chemie (Leipzig), 1985 , vol. 327, # 4 p. 616 - 626
反应条件
Bacillus megaterium ECU1001 epoxide hydrolase in potassium phosphate buffer; dimethyl sulfoxide
T=30°C; pH=7; 0.833333 h; Resolution of racemateEnzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Zhao, Jing; Chu, Yan-Yan; Li, Ai-Tao; Ju, Xin; Kong, Xu-Dong; Pan, Jiang; Tang, Yun; Xu, Jian-He
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 9 p. 1510 - 1518
反应条件
sulfuric acid
1 h; Ambient temperature;
参考文献
Ohta, Hiromichi; Miyamae, Yoshitaka; Tsuchihashi, Gen-ichi
Agricultural and Biological Chemistry, 1989 , vol. 53, # 1 p. 215 - 222
反应条件
3-ethyl-2-chlorobenzoxazolium tetrafluoroborate; tetraethylammonium chloride; triethylamine in dichloromethane
参考文献
Echigo,Y. et al.
Chemistry Letters, 1977 , p. 1013 - 1014
反应条件
(i) K, xylene, (ii) /BRN= 117187/; Multistep reaction;
参考文献
Wyrick; Piantadosi
Journal of Medicinal Chemistry, 1978 , vol. 21, # 4 p. 386 - 390
反应条件
periodic acid in 1,4-dioxane; water
T=55°C; 0.666667 h;
参考文献
Shapenova; Belyatskii; Panicheva
Russian Journal of Organic Chemistry, 2010 , vol. 46, # 7 p. 1017 - 1020
反应条件
1.1: polymer-supported selenium lithium / 20 °C
1.2: tetrahydrofuran / 20 h / 20 °C
1.3: m-chloroperoxybenzoic acid; K2HPO4 / tetrahydrofuran; dimethylformamide / 10 h / 20 °C
2.1: aq. HCl / tetrahydrofuran; dimethylformamide / 65 °C
View Scheme
参考文献
Hu, Qiao-Sheng; Sheng, Shou-Ri; Lin, Shu-Ying; Wei, Mei-Hong; Xin, Qin; Liu, Xiao-Ling
Journal of Chemical Research, 2007 , # 2 p. 74 - 75
反应条件
sodium tetrahydroborate; zirconium tetrachloride; L-proline in tetrahydrofuran
3 h; Ambient temperature;
参考文献
Santosh Laxmi; Iyengar
Synthetic Communications, 1997 , vol. 27, # 10 p. 1731 - 1736
参考文献
Shtacher; Rubinstein; Somani
Journal of Medicinal Chemistry, 1978 , vol. 21, # 7 p. 678 - 683
