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乙二醇
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63148-62-9
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471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
218608-73-2
合成路线
（共 7 条）
218608-72-1
→
反应条件
218608-73-2
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran; dichloromethane T=0°C; 2 h;
参考文献
Mathew, Simon; Imahori, Hiroshi
Journal of Materials Chemistry, 2011 , vol. 21, # 20 p. 7166 - 7174
1440427-06-4
→
反应条件
218608-73-2
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran; dichloromethane T=20°C; 1.5 h; Inert atmosphere;
参考文献
Planells, Miquel; Abate, Antonio; Hollman, Derek J.; Stranks, Samuel D.; Bharti, Vishal; Gaur, Jitender; Mohanty, Dibyajyoti; Chand, Suresh; Snaith, Henry J.; Robertson, Neil
Journal of Materials Chemistry A, 2013 , vol. 1, # 23 p. 6949 - 6960
20440-94-2
4,4-二甲氧基三苯胺
→
反应条件
218608-73-2
反应条件
1: 85 percent / PhI(O2CCF3)2; I2 / CHCl3 2: CuI; Cl2Pd(PPh3)2; TEA 3: K2CO3 / methanol View Scheme
参考文献
Goeransson, Erik; Emanuelsson, Rikard; Jorner, Kjell; Markle, Todd F.; Hammarstroem, Leif; Ottosson, Henrik
Chemical Science, 2013 , vol. 4, # 9 p. 3522 - 3532
201802-15-5
4-碘-4',4''-二甲氧基三苯胺
→
反应条件
218608-73-2
反应条件
1: CuI; Cl2Pd(PPh3)2; TEA 2: K2CO3 / methanol View Scheme
参考文献
Goeransson, Erik; Emanuelsson, Rikard; Jorner, Kjell; Markle, Todd F.; Hammarstroem, Leif; Ottosson, Henrik
Chemical Science, 2013 , vol. 4, # 9 p. 3522 - 3532
696-62-8
4-碘苯甲醚
→
反应条件
218608-73-2
反应条件
1: 50 percent / CuI; t-BuOK; 2,2'-bipyridyl / toluene / 4 h / Heating 2: 85 percent / PhI(O2CCF3)2; I2 / CHCl3 3: CuI; Cl2Pd(PPh3)2; TEA 4: K2CO3 / methanol View Scheme
参考文献
Planells, Miquel; Abate, Antonio; Hollman, Derek J.; Stranks, Samuel D.; Bharti, Vishal; Gaur, Jitender; Mohanty, Dibyajyoti; Chand, Suresh; Snaith, Henry J.; Robertson, Neil
Journal of Materials Chemistry A, 2013 , vol. 1, # 23 p. 6949 - 6960
74497-02-2
→
反应条件
218608-73-2
反应条件
1: 50 percent / CuI; t-BuOK; 2,2'-bipyridyl / toluene / 4 h / Heating 2: 85 percent / PhI(O2CCF3)2; I2 / CHCl3 3: CuI; Cl2Pd(PPh3)2; TEA 4: K2CO3 / methanol View Scheme
参考文献
Lin, Jui-Hsien; Elangovan, Arumugasamy; Ho, Tong-Ing
Journal of Organic Chemistry, 2005 , vol. 70, # 18 p. 7397 - 7407
106-40-1
对溴苯胺
→
反应条件
218608-73-2
反应条件
1: potassium tert-butylate; [2,2']bipyridinyl; copper(l) iodide / toluene / 120 °C / |Inert atmosphere 2: bis-triphenylphosphine-palladium(II) chloride; triphenylphosphine; copper(l) iodide; piperidine / toluene / 90 °C / |Schlenk technique; |Inert atmosphere 3: tetrabutyl ammonium fluoride / dichloromethane; tetrahydrofuran / 1.5 h / 20 °C / |Inert atmosphere View Scheme
参考文献
Planells, Miquel; Abate, Antonio; Hollman, Derek J.; Stranks, Samuel D.; Bharti, Vishal; Gaur, Jitender; Mohanty, Dibyajyoti; Chand, Suresh; Snaith, Henry J.; Robertson, Neil
Journal of Materials Chemistry A, 2013 , vol. 1, # 23 p. 6949 - 6960
