Journal of the American Chemical Society, , vol. 77, p. 5562,5577
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反应条件
1: 1-((2-bromovinyl)dimethylsiloxy)-4-t-butylcyclohexane With 2,2'-azo-bisisobutyronitrile; n-Bu3SnD in octane; benzene 5 h; Heating; 2: With potassium fluoride; dihydrogen peroxide; potassium hydrogencarbonate in tetrahydrofuran; methanol; water T=20°C; 3: benzoyl chloride With pyridine in acetonitrile T=20°C; 20 h; Further byproducts given. Title compound not separated from byproducts;
