6-甲基-7-氧杂双环[4.1.0]庚烷-2-酮合成路线 (共 22 条)
反应条件
hydrogenchloride; lithium diisopropyl amide
1.) THF, -23 deg C, 2 h, 2.) EtOH, 60 deg C, 30 min; Yield given. Multistep reaction;
参考文献
Wender, Paul A.; Erhardt, Jeanette M.; Letendre, Leo J.
Journal of the American Chemical Society, 1981 , vol. 103, # 8 p. 2114 - 2116
反应条件
1: 49 percent / HCl / 0 °C
2: H2/PtO2 / methanol
3: diethyl peroxide, Ph3P / 220 °C / 5 Torr / other methylcyclohexanol cis-diols
View Scheme
参考文献
Robinson, Philip L.; Evans, Slayton A.
Journal of Organic Chemistry, 1985 , vol. 50, # 20 p. 3860 - 3863