(2-氨基-2-硫氧代乙基)甲基氨基甲酸叔丁酯合成路线 （共 2 条）
反应条件
1: With Lawesson's reagent in tetrahydrofuran T=0 - 20°C; 12 h; 2: With sodium hydrogencarbonate in water
参考文献
Takeda Pharmaceutical Company Limited
Patent: US2009/156642 A1, 2009 ;
Location in patent: Page/Page column 41; 42 ;
反应条件
1: 72 percent / diisopropylethylamine / CH2Cl2 / 0 - 20 °C 2: 65 percent / P2S5; NaHCO3 / 1,2-dimethoxy-ethane / 48 h / 0 - 20 °C View Scheme
参考文献
Harnett, Jeremiah J.; Roubert, Veronique; Dolo, Christine; Charnet, Christelle; Spinnewyn, Brigitte; Cornet, Sylvie; Rolland, Alain; Marin, Jean-Gregoire; Bigg, Dennis; Chabrier, Pierre-E.
Bioorganic and Medicinal Chemistry Letters, 2004 , vol. 14, # 1 p. 157 - 160
