2,6-二甲基-苯甲酰氯合成路线 （共 23 条）
参考文献
Yates, Keith; Mandrapilias, George
Journal of Organic Chemistry, 1980 , vol. 45, # 19 p. 3892 - 3902
参考文献
Bowman, W. Russell; Forshaw, J. Anthony; Hall, Kevin P.; Kitchin, Jonathan P.; Mott, Andrew W.
Tetrahedron, 1996 , vol. 52, # 11 p. 3961 - 3972
参考文献
Bowman, W. Russell; Forshaw, J. Anthony; Hall, Kevin P.; Kitchin, Jonathan P.; Mott, Andrew W.
Tetrahedron, 1996 , vol. 52, # 11 p. 3961 - 3972
反应条件
1: 1) diazotation
2: thionyl chloride
View Scheme
参考文献
Yates, Keith; Mandrapilias, George
Journal of Organic Chemistry, 1980 , vol. 45, # 19 p. 3892 - 3902
反应条件
1: aq. H2SO4 / Heating
2: SOCl2
View Scheme
参考文献
Haering,M.
Helvetica Chimica Acta, 1960 , vol. 43, p. 104 - 113
参考文献
Marion Laboratories, Inc.
Patent: US4022900 A1, 1977 ;
反应条件
in tetrahydrofuran
2 h;
参考文献
Lehmann, Fredrik; Currier, Erika A.; Olsson, Roger; Hacksell, Uli; Luthman, Kristina
Bioorganic and Medicinal Chemistry, 2005 , vol. 13, # 8 p. 3057 - 3068
反应条件
1: 98 percent / H2SO4 / toluene / 4 h / Heating
2: 99 percent / Na2CO3, H2O / 4 h / Heating
3: 36 percent / CrO3, CH3COOH / 2 h / 20 °C
View Scheme
参考文献
Adolphe-Pierre; Menager; Tombret; Verite; Lepage; Lafont
Farmaco, 1998 , vol. 53, # 7 p. 513 - 518
反应条件
1: diethyl ether
2: 1.) PCl5, 2.) potassium tert-butoxide / 2.) DMSO
View Scheme
参考文献
Yates, Keith; Mandrapilias, George
Journal of Organic Chemistry, 1980 , vol. 45, # 19 p. 3892 - 3902
反应条件
1: 98 percent / H2SO4 / toluene / 4 h / Heating
2: 99 percent / Na2CO3, H2O / 4 h / Heating
3: 12 percent / sodium persulfate, sodium acetate, copper(II) acetate monohydrate, CH3COOH / 8 h / Heating
View Scheme
参考文献
Adolphe-Pierre; Menager; Tombret; Verite; Lepage; Lafont
Farmaco, 1998 , vol. 53, # 7 p. 513 - 518
