3-(3-氯苯基)-2-丁酮合成路线 （共 6 条）
反应条件
(i) NaOiPr, iPrOH, (ii) /BRN= 969135/; Multistep reaction;
参考文献
Rodriguez, Cristina; Gonzalo, Gonzalo de; Torres Pazmino, Daniel E.; Fraaije, Marco W.; Gotor, Vicente
Tetrahedron Asymmetry, 2009 , vol. 20, # 10 p. 1168 - 1173
反应条件
1: NH4OAc / acetic acid / 3 h / Heating 2: Fe, FeCl3, aq. HCl / 1 h / Heating 3: (i) NaOiPr, iPrOH, (ii) /BRN= 969135/ View Scheme
参考文献
Binovic,K.; Vrancea,S.
Chimica Therapeutica, 1968 , vol. 3, p. 313 - 320
反应条件
(i) Li, (ii) /BRN= 102413/, (iii) aq. Na2Cr2O7, H2SO4; Multistep reaction;
参考文献
Stang,P.J.; Dueber,T.E.
Journal of the American Chemical Society, 1977 , vol. 99, # 8 p. 2602 - 2610
反应条件
1: Fe, FeCl3, aq. HCl / 1 h / Heating 2: (i) NaOiPr, iPrOH, (ii) /BRN= 969135/ View Scheme
参考文献
Binovic,K.; Vrancea,S.
Chimica Therapeutica, 1968 , vol. 3, p. 313 - 320
反应条件
formic acid; formamide T=170 - 180°C; 16 h;
参考文献
Binovic,K.; Vrancea,S.
Chimica Therapeutica, 1968 , vol. 3, p. 313 - 320
反应条件
1: hydroxylamine hydrochloride; sodium hydroxide / ethanol; water / 1 h / Reflux 2: pyridine / 2 h / Cooling with ice 3: water; N,N-dimethyl-aniline / acetonitrile / 25 °C View Scheme
参考文献
Yamamoto, Yutaro; Hasegawa, Hiroto; Yamataka, Hiroshi
Journal of Organic Chemistry, 2011 , vol. 76, # 11 p. 4652 - 4660
