in dichloromethane
addn. of chlorine to a suspn. of SbPh2F at -97°C, warming to -40°C; evapn., crystn., elem. anal.;
参考文献
Bone, Stephen P.; Begley, Michael J.; Sowerby, D. Bryan
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1992 , # 13 p. 2085 - 2092
in tetrahydrofuran
Zr complex dissolved in THF; Ph2SbCl3 (1 equiv.) added at room temp.; stirred; volatiles removed in vac.; crystd. from hexane at 5°C (Ph2SbCl); detd. by single crystal X-ray diffraction;
参考文献
Fish, Cheryl; Green, Michael; Kilby, Richard J.; McGrady, John E.; Pantazis, Dimitrios A.; Russell, Christopher A.
Dalton Transactions, 2008 , # 28 p. 3753 - 3758
in tetrahydrofuran
in foil wrapped tube; Zr complex and MeN(CO)2CHCH (1 equiv.) dissolved in THF; Ph2SbCl3 (1 equiv.) added; stirred for 3 h; crystd. from hexane at 5°C (Ph2SbCl); detd. by single crystal X-ray diffraction;
参考文献
Fish, Cheryl; Green, Michael; Kilby, Richard J.; McGrady, John E.; Pantazis, Dimitrios A.; Russell, Christopher A.
Dalton Transactions, 2008 , # 28 p. 3753 - 3758
