2-(甲基亚硫酰基)吡啶合成路线 （共 42 条）
反应条件
methylmagnesium bromide in tetrahydrofuran 0.25 h; Ambient temperature;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 62, # 12 p. 3848 - 3850
反应条件
n-butyllithium 1) Et2O or THF, -78 deg C; Yield given. Multistep reaction;
参考文献
Uenishi; Tanaka; Wakabayashi; Oae; Tsukube
Tetrahedron Letters, 1990 , vol. 31, # 32 p. 4625 - 4628
反应条件
in tetrahydrofuran 0.25 h; Ambient temperature;
参考文献
Phosphorus and Sulfur and the Related Elements, , vol. 34, p. 123 - 132
反应条件
in tert-butyl alcohol 5 h; Heating;
参考文献
Furukawa, Naomichi; Ogawa, Satoshi; Kawai, Tsutomu; Oae, Shigeru
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 8 p. 1839 - 1845
反应条件
methylmagnesium bromide in tetrahydrofuran 0.25 h; Ambient temperature;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 62, # 12 p. 3848 - 3850
反应条件
in tetrahydrofuran Ambient temperature;
参考文献
Oae, Shigeru; Kawai, Tsutomu; Furukawa, Naomichi; Iwasaki, Fujiko
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1987 , p. 405 - 412
Title/Abstract Full Text Show Details
Kawai, Tsutomu; Kodera, Yoichi; Furukawa, Naomichi; Oae, Shigeru; Ishida, Masahiro; et al.
Phosphorus and Sulfur and the Related Elements, 1987 , vol. 34, p. 139 - 148
反应条件
1: 7 percent Spectr. / 2-methyl-propan-2-ol / 5 h / Heating 2: 93 percent / hydrogen peroxide 3: 79 percent Spectr. / ethanol / 1.5 h / Heating View Scheme
参考文献
Furukawa, Naomichi; Ogawa, Satoshi; Kawai, Tsutomu; Oae, Shigeru
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 8 p. 1839 - 1845
反应条件
in ethanol 2 h; HeatingSelective ipso-substitution of CH3SO group directly bound to 2 or 4 position in pyridine ring by several nucleophiles; Product distribution;
参考文献
Tetrahedron Letters, , vol. 24, # 31 p. 3243 - 3246
反应条件
1: 7 percent Spectr. / 2-methyl-propan-2-ol / 5 h / Heating 2: 93 percent / hydrogen peroxide View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 8 p. 1839 - 1845
反应条件
glucose-6-phosphate dehydrogenase; Glc 6P; recombinant 4-hydroxyacetophenone monooxygenase; dimethyl sulfoxide; NADPH T=20°C; pH=8 - 10.5; 0.5 h; aq. bufferEnzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
European Journal of Organic Chemistry, , # 33 p. 6409 - 6416
