2-(甲基亚硫酰基)吡啶合成路线 （共 42 条）
反应条件
sodium tetrahydroborate; titanium tetrachloride in ethylene glycol dimethyl ether 0.5 h; Ambient temperature;
参考文献
Kano, Shinzo; Tanaka, Yasuyuki; Sugino, Eiichi; Hibino, Sstoshi
Synthesis, 1980 , # 9 p. 695 - 697
反应条件
in ethanol T=50°C; 5 h;
参考文献
Tetrahedron Letters, , vol. 24, # 31 p. 3243 - 3246
反应条件
ethyl mercaptan sodium salt in ethanol T=50°C; 5 h;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 8 p. 1839 - 1845
反应条件
in tert-butyl alcohol 5 h; Heating;
参考文献
Tetrahedron Letters, , vol. 24, # 31 p. 3243 - 3246
反应条件
in ethanol 2 h; HeatingSelective ipso-substitution of CH3SO group directly bound to 2 or 4 position in pyridine ring by several nucleophiles; Product distribution;
参考文献
Tetrahedron Letters, , vol. 24, # 31 p. 3243 - 3246
反应条件
3-chloro-benzenecarboperoxoic acid in dichloromethane
T=0°C; 16 h;
参考文献
Hendriks, Christine M. M.; Lamers, Philip; Engel, Julien; Bolm, Carsten
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 17 p. 3363 - 3368
反应条件
1: 67 percent Chromat. / triethylamine / acetonitrile / Ambient temperature; overnight
2: 22 percent / acetic acid / methanol / 3 h / 45 °C
View Scheme
参考文献
Furukawa, Naomichi; Takahashi, Fujio; Tsutomu, Kawai; Kishimoto, Keiko; Ogawa, Satoshi; Oae, Shigeru
Phosphorus and Sulfur and the Related Elements, 1983 , vol. 16, p. 167 - 180
反应条件
sodium ethanolate in acetonitrile
Ambient temperature;
参考文献
Furukawa, Naomichi; Konno, Yasuo; Tsuruoka, Masayuki; Fujihara, Hisashi; Ogawa, Satoshi
Chemistry Letters, 1989 , p. 1501 - 1504
反应条件
sodium ethanolate in acetonitrile
Ambient temperature;
参考文献
Furukawa, Naomichi; Konno, Yasuo; Tsuruoka, Masayuki; Fujihara, Hisashi; Ogawa, Satoshi
Chemistry Letters, 1989 , p. 1501 - 1504
反应条件
acetic acid in methanol
T=45°C; 3 h;
参考文献
Furukawa, Naomichi; Takahashi, Fujio; Tsutomu, Kawai; Kishimoto, Keiko; Ogawa, Satoshi; Oae, Shigeru
Phosphorus and Sulfur and the Related Elements, 1983 , vol. 16, p. 167 - 180
