3,5-二甲氧基二苯乙烯合成路线 (共 10 条)
反应条件
boron tribromide in dichloromethane T=-78°C; 12 h;
参考文献
Kabir, M. Shahjahan; Engelbrecht, Kathleen; Polanowski, Rebecca; Krueger, Sarah M.; Ignasiak, Rachel; Rott, Marc; Schwan, William R.; Stemper, Mary E.; Reed, Kurt D.; Sherman, David; Cook, James M.; Monte, Aaron
Bioorganic and Medicinal Chemistry Letters, 2008 , vol. 18, # 21 p. 5745 - 5749
反应条件
boron tribromide in dichloromethane T=0 - 20°C;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 40, # 5 p. 1130 - 1136
反应条件
oxygen in 1,2-dichloro-ethane Ambient temperatureIrradiation; Product distribution;
参考文献
Journal of Organic Chemistry, , vol. 61, # 22 p. 7793 - 7800
反应条件
1: 51 percent / BBr3 / CH2Cl2 / 0 - 20 °C 2: 97 percent / H2 / 10percent Pd/C / ethanol / 1 h View Scheme
参考文献
Ali; Kondo; Tsuda
Chemical and Pharmaceutical Bulletin, 1992 , vol. 40, # 5 p. 1130 - 1136
反应条件
1: 43 percent / BBr3 / CH2Cl2 / 0 - 20 °C 2: 99 percent / H2 / 10percent Pd/C / ethanol / 1 h View Scheme
参考文献
Ali; Kondo; Tsuda
Chemical and Pharmaceutical Bulletin, 1992 , vol. 40, # 5 p. 1130 - 1136
反应条件
pyridine hydrochloride T=190°C; 4 h;
参考文献
Xia, Likai; Lee, Yong Rok
Synlett, 2008 , # 11 p. 1643 - 1646
反应条件
boron tribromide in dichloromethane T=0 - 20°C;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 40, # 5 p. 1130 - 1136
反应条件
diethyl ether; platinum
Hydrogenation;
参考文献
Fang, Jim-Min; Su, Wen-Chiung; Cheng, Yu-Shia
Phytochemistry (Elsevier), 1988 , vol. 27, # 5 p. 1395 - 1398
反应条件
in acetonitrile
UV-irradiation; Title compound not separated from byproducts;
参考文献
Roberts, Jeffrey C.; Pincock, James A.
Journal of Organic Chemistry, 2004 , vol. 69, # 12 p. 4279 - 4282
反应条件
T=25°C; 0.0333333 h; UV-irradiation; Title compound not separated from byproducts;
参考文献
Roberts, Jeffrey C.; Pincock, James A.
Journal of Organic Chemistry, 2006 , vol. 71, # 4 p. 1480 - 1492