N-对甲苯磺酰-L-丙氨酸合成路线 (共 10 条)
反应条件
sodium hydroxide in diethyl ether; water T=20°C;
参考文献
Ghosh, Debashis; Sahu, Debashis; Saravanan; Abdi, Sayed H. R.; Ganguly, Bishwajit; Khan, Noor-Ul H.; Kureshy, Rukhsana I.; Bajaj, Hari C.
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 21 p. 3451 - 3460
反应条件
ozone in dichloromethane
参考文献
Tetrahedron Letters, , vol. 32, # 11 p. 1467 - 1470
反应条件
1: 80 percent / -70 °C 2: Ti(OiPr)4, L-(+)-DIPT, TBHP, CaH2, silica gel / CH2Cl2 / 48 h / Ambient temperature 3: O3 / CH2Cl2 View Scheme
参考文献
Tetrahedron Letters, , vol. 32, # 11 p. 1467 - 1470
反应条件
1: Ti(OiPr)4, L-(+)-DIPT, TBHP, CaH2, silica gel / CH2Cl2 / 48 h / Ambient temperature 2: O3 / CH2Cl2 View Scheme
参考文献
Tetrahedron Letters, , vol. 32, # 11 p. 1467 - 1470
反应条件
sodium hydroxide; diethyl ether
参考文献
Chemische Berichte, , vol. 48, p. 374
反应条件
sulfuric acid T=60 - 70°C;
参考文献
Seong, Mi Ra; Lee, Hong Jung; Kim, Jae Nyoung
Tetrahedron Letters, 1998 , vol. 39, # 34 p. 6219 - 6222
反应条件
sulfuric acid
T=60 - 70°C; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Seong, Mi Ra; Lee, Hong Jung; Kim, Jae Nyoung
Tetrahedron Letters, 1998 , vol. 39, # 34 p. 6219 - 6222
反应条件
sulfuric acid
T=60 - 70°C; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Seong, Mi Ra; Lee, Hong Jung; Kim, Jae Nyoung
Tetrahedron Letters, 1998 , vol. 39, # 34 p. 6219 - 6222
反应条件
chloro-trimethyl-silane in chloroform
6 h; Heating;
参考文献
Shipov, A. G.; Orlova, N. A.; Novikova, O. P.; Baukov, Yu. I.
J. Gen. Chem. USSR (Engl. Transl.), 1985 , vol. 55, # 4 p. 943 - 944,841 - 842
反应条件
chloro-trimethyl-silane in chloroform
6 h; Heating;
参考文献
Shipov, A. G.; Orlova, N. A.; Kobzareva, V. P.; Mozzhukhin, A. O.; Antipin, M. Yu.; et al.
Russian Journal of General Chemistry, 1993 , vol. 63, # 2.2 p. 262 - 266
Zhurnal Obshchei Khimii, 1993 , vol. 63, # 2 p. 371 - 377