5-氧代-1-[(对甲苯基)磺酰基]-L-脯氨酸合成路线 (共 9 条)
反应条件
diisopropyl-carbodiimide in acetonitrile T=-5 - 50°C;
参考文献
SOLVAY (Societe Anonyme)
Patent: WO2009/80708 A1, 2009 ;
Location in patent: Page/Page column 4-5 ;
反应条件
acetyl chloride 2 h; Heating;
参考文献
Srikanth; Kumar; Ghosh, Balaram; Jha, Tarun
Bioorganic and Medicinal Chemistry, 2002 , vol. 10, # 7 p. 2119 - 2131
反应条件
1: 69.3 percent / aq. NaOH / 70 °C 2: 74.46 percent / acetyl chloride / 2 h / Heating View Scheme
参考文献
Rudinger et al.
Collection of Czechoslovak Chemical Communications, 1959 , vol. 24, p. 2013,2014,2016
反应条件
1: 69.3 percent / aq. NaOH / 70 °C 2: 74.46 percent / acetyl chloride / 2 h / Heating View Scheme
参考文献
Rudinger et al.
Collection of Czechoslovak Chemical Communications, 1959 , vol. 24, p. 2013,2014,2016
参考文献
Harington; Moggridge
Journal of the Chemical Society, 1940 , p. 706,712
反应条件
1: brucine 2: aqueous NaOH / anschliessend mit Natrium und NH3 View Scheme
参考文献
Rudinger; Czurbova
Collection of Czechoslovak Chemical Communications, 1954 , vol. 19, p. 386,390
反应条件
1: water; NH3 2: aqueous HBr; acetic acid; phenol View Scheme
参考文献
Rudinger et al.
Collection of Czechoslovak Chemical Communications, 1959 , vol. 24, p. 2013,2014,2016
参考文献
Swan
Pr. int. Wool Textile Res. Conf. Australia, 1955 , p. C. 175, 179
反应条件
2: sodium; liquid NH3
View Scheme
参考文献
Rudinger
Collection of Czechoslovak Chemical Communications, 1954 , vol. 19, p. 365,373