2-氯-4-甲氧基苯乙酮合成路线 （共 91 条）
反应条件
hydrogenchloride; ammonium nitrate; iodine; oxygen in water; acetonitrile T=60°C; 24 h; Green chemistry; regioselective reaction;
参考文献
Advanced Synthesis and Catalysis, , vol. 356, # 6 p. 1266 - 1274
反应条件
chlorine dioxide in tetrachloromethane T=52 - 54°C; 1.16667 h; Further byproducts given. Title compound not separated from byproducts;
参考文献
Polish Journal of Chemistry, , vol. 60, # 7-12 p. 811 - 824
反应条件
chlorine dioxide in tetrachloromethane T=52 - 54°C; 1.16667 h; Further byproducts given;
参考文献
Polish Journal of Chemistry, , vol. 60, # 7-12 p. 811 - 824
反应条件
water; sodium chloride T=75°C; 0.833333 h; microwave irradiation;
参考文献
Utsukihara, Takamitsu; Nakamura, Hiroaki; Watanabe, Masashige; Akira Horiuchi
Tetrahedron Letters, 2006 , vol. 47, # 52 p. 9359 - 9364
反应条件
1: 87 percent / LDA / tetrahydrofuran / 0.5 h / -65 °C 2: 60 percent / EtMgBr / tetrahydrofuran / 2 h / -70 - -40 °C View Scheme
参考文献
Tetrahedron, , vol. 51, # 3 p. 703 - 710
反应条件
1: 0.2M ammonium nitrate / methanol; H2O / cathodic reduction 2: 5M KOH / ethanol / Heating 3: cond. H2SO4 / H2O; dioxane / 3 h / Ambient temperature View Scheme
参考文献
Tetrahedron Letters, , vol. 23, # 15 p. 1609 - 1612
反应条件
1: 5M KOH / ethanol / Heating 2: cond. H2SO4 / H2O; dioxane / 3 h / Ambient temperature View Scheme
参考文献
Tetrahedron Letters, , vol. 23, # 15 p. 1609 - 1612
反应条件
1: 90 percent / CHCl3; dimethylformamide / cathodic reduction 2: 90 percent / NaH / tetrahydrofuran / 1 h / 0 °C 3: 0.2M ammonium nitrate / methanol; H2O / cathodic reduction 4: 5M KOH / ethanol / Heating 5: cond. H2SO4 / H2O; dioxane / 3 h / Ambient temperature View Scheme
参考文献
Tetrahedron Letters, , vol. 23, # 15 p. 1609 - 1612
反应条件
carbon disulfide; aluminium trichloride in der Kaelte;
参考文献
Chemische Berichte, , vol. 50, p. 417
Journal of the Chemical Society, , vol. 97, p. 2520
反应条件
trifluorormethanesulfonic acid 264 h; Ambient temperature;
参考文献
Booth, Brian L.; Noori, Ghazi F.M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 2894 - 2900
