2-氯-4-甲氧基苯乙酮合成路线 (共 91 条)
参考文献
Tutin
Journal of the Chemical Society, 1910 , vol. 97, p. 2520
反应条件
1: [Ru(II)(2,2’-bipyridine)3]Cl2; DNP; ascorbic acid powder / methanol; water / 15 h / Inert atmosphere; Irradiation 2: bromine / chloroform / 0 - 65 °C View Scheme
参考文献
Maji, Tapan; Karmakar, Ananta; Reiser, Oliver
Journal of Organic Chemistry, 2011 , vol. 76, # 2 p. 736 - 739
反应条件
aluminium trichloride 14 h; Ambient temperature;
参考文献
Overacre, Lynette B.; Magarian, Robert A.
Bioorganic Chemistry, 1998 , vol. 26, # 1 p. 15 - 31
参考文献
Ando
Yuki Gosei Kagaku Kyokaishi, 1959 , vol. 17, p. 777,779
Chem.Abstr., 1960 , p. 4492
反应条件
[bmim]Br T=20°C; 0.666667 h;
参考文献
Kamal, Ahmed; Chouhan, Gagan
Tetrahedron Letters, 2004 , vol. 45, # 48 p. 8801 - 8805
反应条件
aluminium trichloride in n-heptane 2.5 h; Heating;
参考文献
Kraus, Michael; Biskup, Ellen; Richling, Elke; Schreier, Peter
Journal of Labelled Compounds and Radiopharmaceuticals, 2006 , vol. 49, # 13 p. 1151 - 1162
参考文献
Kamal, Ahmed; Chouhan, Gagan
Tetrahedron Letters, 2005 , vol. 46, # 9 p. 1489 - 1491
反应条件
1: 3-methoxy-benzenethiol With sodium methylate in methanol T=35°C; 2: 4-methoxyphenyl chloromethyl ketone in methanol T=0 - 35°C; 1.16667 h;
参考文献
BASF AKTIENGESELLSCHAFT
Patent: WO2005/42477 A1, 2005 ;
Location in patent: Page/Page column 4 ;
反应条件
in tetrahydrofuran 16 h; Ambient temperature;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1373 - 1380
反应条件
1: 9.5 g / AlCl3 / heptane / 2.5 h / Heating 2: 40 percent / triethylamine / acetonitrile / 3 h / Heating 3: 75 percent / 2 h / 100 °C 4: hydrogen chloride; methanol / ethyl acetate / 24 h / 20 °C 5: potassium hydroxide / methanol; H2O / 1 h / 0 - 4 °C View Scheme
参考文献
Kraus, Michael; Biskup, Ellen; Richling, Elke; Schreier, Peter
Journal of Labelled Compounds and Radiopharmaceuticals, 2006 , vol. 49, # 13 p. 1151 - 1162