4-甲酰基-2-甲氧基苯甲腈合成路线 （共 4 条）
反应条件
zinc cyanide; tetrakis(triphenylphosphine) palladium(0) in DMF (N,N-dimethyl-formamide) T=110°C; 4 h;
参考文献
ENDORECHERCHE, INC.
Patent: WO2005/66194 A1, 2005 ;
Location in patent: Page/Page column 161 ;
WO 2005/066194 A1
反应条件
tetrakis(triphenylphosphine) palladium(0) in N,N-dimethyl-formamide T=110°C; 8 h;
参考文献
MERCK SHARP and DOHME CORP.; PASTERNAK, Alexander; BLIZZARD, Timothy; CHOBANIAN, Harry; DE JESUS, Reynalda; DING, Fa-Xiang; DONG, Shuzhi; GUDE, Candido; KIM, Dooseop; TANG, Haifeng; WALSH, Shawn; PIO, Barbara; JIANG, Jinlong
Patent: WO2013/28474 A1, 2013 ;
Location in patent: Page/Page column 79 ;
反应条件
1: potassium carbonate / N,N-dimethyl-formamide / 8 h 2: tetrakis(triphenylphosphine) palladium(0) / N,N-dimethyl-formamide / 8 h / 110 °C View Scheme
参考文献
MERCK SHARP and DOHME CORP.; PASTERNAK, Alexander; BLIZZARD, Timothy; CHOBANIAN, Harry; DE JESUS, Reynalda; DING, Fa-Xiang; DONG, Shuzhi; GUDE, Candido; KIM, Dooseop; TANG, Haifeng; WALSH, Shawn; PIO, Barbara; JIANG, Jinlong
Patent: WO2013/28474 A1, 2013 ;
反应条件
pyridine hydrochloride
0.5 h; Heating / reflux;
参考文献
ENDORECHERCHE, INC.
Patent: WO2005/66194 A1, 2005 ;
Location in patent: Page/Page column 162 ;
WO 2005/066194 A1
