反应条件
1: TBAF
2: 1.) LDA, HMPA / 1.) THF, -78 deg C
3: H2 / Lindlar catalyst
4: 48percent HBr / methanol
5: 96 percent / O2, NaHCO3 / methanol
6: 47 percent / 70percent HClO4 / CH2Cl2; tetrahydrofuran
View Scheme
参考文献
Fukuyama; Kiriyama; Kodama; Iwaki; Hosozawa; Aki; Matsui
Chemical and Pharmaceutical Bulletin, 1994 , vol. 42, # 10 p. 2211 - 2213
