4-氯-4'-硝基二苯硫醚合成路线 （共 18 条）
反应条件
potassium carbonate in N,N-dimethyl-formamide T=80°C; 9 h;
参考文献
Bandna; Guha, Nitul Ranjan; Shil, Arun K.; Sharma, Dharminder; Das, Pralay
Tetrahedron Letters, 2012 , vol. 53, # 39 p. 5318 - 5322
反应条件
ReOBr2(hmpbta)(PPh3); 4,4,5,5-tetramethyl-[1,3,2]dioxaborolane in tetrahydrofuran 1 h; Reflux; Reagent/catalystTime; chemoselective reaction;
参考文献
Sousa, Sara C. A.; Bernardo, Joana R.; Wolff, Mariusz; Machura, Barbara; Fernandes, Ana C.
European Journal of Organic Chemistry, 2014 , vol. 2014, # 9 p. 1855 - 1859
反应条件
4,4'-bis(trimethylaminomethyl)-2,2'-bipyridine dihydrobromide; FeCl3·6H2O; potassium hydroxide in water 24 h; Reflux;
参考文献
Wu, Wei-Yi; Wang, Jui-Chan; Tsai, Fu-Yu
Green Chemistry, 2009 , vol. 11, # 3 p. 326 - 329
反应条件
nanoferrite-dopamine copper catalyst in isopropyl alcohol T=120°C; P=517.162 - 3102.97 Torr; 0.416667 h; Microwave irradiation;
参考文献
Nasir Baig; Varma, Rajender S.
Green Chemistry, 2013 , vol. 15, # 2 p. 398 - 417
反应条件
[Me2N]3P=NP(=NEt)[NMe2]2; copper(I) bromide in toluene Substitution; Heating;
参考文献
Palomo, Claudio; Oiarbide, Mikel; Lopez, Rosa; Gomez-Bengoa, Enrique
Tetrahedron Letters, 2000 , vol. 41, # 8 p. 1283 - 1286
反应条件
tetrabutyl ammonium fluoride in acetonitrile T=25°C; 5 h; Microwave irradiation;
参考文献
Liu, Chuanzhi; Zang, Xufeng; Yu, Baohua; Yu, Xiaochun; Xu, Qing
Synlett, 2011 , # 8 art. no. W03511ST, p. 1143 - 1148
反应条件
iron; potassium carbonate in dimethyl sulfoxide; N,N-dimethyl-formamide T=120°C; 18 h; Inert atmosphere;
参考文献
Li, Yaming; Nie, Caiping; Wang, Huifeng; Li, Xiaoying; Verpoort, Francis; Duan, Chunying
European Journal of Organic Chemistry, 2011 , # 36 p. 7331 - 7338
反应条件
1: copper(l) iodide; Na2S*9H2O; sulfur / N,N-dimethyl-formamide / 15 h / 80 °C / Inert atmosphere 2: iron; potassium carbonate / dimethyl sulfoxide; N,N-dimethyl-formamide / 18 h / 120 °C / Inert atmosphere View Scheme
参考文献
European Journal of Organic Chemistry, , # 36 p. 7331 - 7338
反应条件
in N,N-dimethyl-formamide T=120°C;
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 14, # 4 p. 1053 - 1056
参考文献
Magnetic Resonance in Chemistry, , vol. 25, p. 1001 - 1006
