1-甲基-2-丙烯基氯化镁合成路线 （共 21 条）
反应条件
in tetrahydrofuran
1.) -30 deg C, 1 h, 2.) -30 deg C to room temp.;
参考文献
Dubois, Jacques-Emile; Lion, Claude; Arouisse, Abdelmajid
Bulletin des Societes Chimiques Belges, 1984 , vol. 93, # 12 p. 1083 - 1088
反应条件
in diethyl ether
T=90°C; 48 h; Yield given;
参考文献
Lehmkuhl, Herbert; Hauschild, Klaus; Bellenbaum, Marita
Chemische Berichte, 1984 , vol. 117, # 1 p. 383 - 388
反应条件
hydrogenchloride
1.) (C2H5)2O, 48 h, 90 deg C, 2.) (C2H5)2O; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Lehmkuhl, Herbert; Hauschild, Klaus; Bellenbaum, Marita
Chemische Berichte, 1984 , vol. 117, # 1 p. 383 - 388
反应条件
hydrogenchloride
1.) (C2H5)2O, 48 h, 90 deg C, 2.) (C2H5)2O; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Lehmkuhl, Herbert; Hauschild, Klaus; Bellenbaum, Marita
Chemische Berichte, 1984 , vol. 117, # 1 p. 383 - 388
反应条件
in diethyl ether
T=-78°C; 0.5 h;
参考文献
Yamamoto, Yoshinori; Nishii, Shinji
Journal of Organic Chemistry, 1988 , vol. 53, # 15 p. 3597 - 3603
参考文献
Lehmkuhl,H. et al.
Justus Liebigs Annalen der Chemie, 1975 , p. 119 - 144
反应条件
in tetrahydrofuran
Yield given. Yields of byproduct given;
参考文献
Laycock, Bronwyn; Kitching, William; Wickham, Geoffrey
Tetrahedron Letters, 1983 , vol. 24, # 51 p. 5785 - 5788
反应条件
(i), (ii) D2O; Multistep reaction;
参考文献
Lehmkuhl,H. et al.
Justus Liebigs Annalen der Chemie, 1975 , p. 119 - 144
反应条件
in tetrahydrofuran
T=-40 - 10°C; 1 h;
参考文献
Bourgain-Commercon, Monique; Normant, Jean F.
Bulletin de la Societe Chimique de France, 1980 , vol. 2, # 5-6 p. 289 - 294
参考文献
Wolf,H. et al.
Chemische Berichte, 1976 , vol. 109, p. 41 - 57
