2,3-二甲基萘-1,4-二酮合成路线 （共 85 条）
反应条件
in acetic acid
0.5 h; Heatingcompetition reaction with alkyl iodides; also with DMSO; Product distribution;
参考文献
Coppa, F.; Fontana, F.; Minisci, F.; Barbosa, M. C. Nogueira; Vismara, E.
Tetrahedron, 1991 , vol. 47, # 35 p. 7343 - 7352
反应条件
sulfuric acid; dihydrogen peroxide
12 h; Heatingother acids; Product distributionMechanism;
参考文献
Coppa, F.; Fontana, F.; Minisci, F.; Barbosa, M. C. Nogueira; Vismara, E.
Tetrahedron, 1991 , vol. 47, # 35 p. 7343 - 7352
反应条件
entsteht noch das Pyrazolinderivat;
参考文献
Bergmann; Bergmann
Journal of Organic Chemistry, 1938 , vol. 3, p. 125,131
反应条件
in benzene
Irradiationat different concentrations of the reagent; Product distribution;
参考文献
Osuka, Atsuhiro; Suzuki, Hitomi; Maruyama, Kazuhiro
Chemistry Letters, 1981 , p. 201 - 204
反应条件
1: 84 percent / NBS, (C6H5CO)2O2 / CCl4
2: 44 percent / H2O / dioxane / 5 h / Heating
View Scheme
参考文献
Lin; Antonini; Cosby; Sartorelli
Journal of Medicinal Chemistry, 1984 , vol. 27, # 6 p. 813 - 815
反应条件
1: 84 percent / NBS, (C6H5CO)2O2 / CCl4
2: 71 percent / acetonitrile / Ambient temperature
View Scheme
参考文献
Lin; Antonini; Cosby; Sartorelli
Journal of Medicinal Chemistry, 1984 , vol. 27, # 6 p. 813 - 815
反应条件
1: 84 percent / NBS, (C6H5CO)2O2 / CCl4
2: 77 percent / acetonitrile / 48 h
View Scheme
参考文献
Lin; Antonini; Cosby; Sartorelli
Journal of Medicinal Chemistry, 1984 , vol. 27, # 6 p. 813 - 815
反应条件
1: 84 percent / NBS, (C6H5CO)2O2 / CCl4
2: 0.9 g / methanol / 72 h / Heating
View Scheme
参考文献
Lin; Antonini; Cosby; Sartorelli
Journal of Medicinal Chemistry, 1984 , vol. 27, # 6 p. 813 - 815
反应条件
1: 84 percent / NBS, (C6H5CO)2O2 / CCl4
2: 44 percent / H2O / dioxane / 5 h / Heating
3: 66 percent / CHCl3 / 24 h / Heating
View Scheme
参考文献
Lin; Antonini; Cosby; Sartorelli
Journal of Medicinal Chemistry, 1984 , vol. 27, # 6 p. 813 - 815
反应条件
1: 84 percent / NBS, (C6H5CO)2O2 / CCl4
2: 44 percent / H2O / dioxane / 5 h / Heating
3: 1.37 g / CHCl3 / 72 h / Heating
View Scheme
参考文献
Lin; Antonini; Cosby; Sartorelli
Journal of Medicinal Chemistry, 1984 , vol. 27, # 6 p. 813 - 815
