反应条件
1: 2-methoxy-5-bromo-pyridine With tris-(dibenzylideneacetone)dipalladium(0); (1-Ad)2P(O)H in tetrahydrofuran
Kumada-Corriu coupling reaction; 0.0833333 h; Inert atmosphere;
2: (pyridin-2-yl)magnesium bromide in tetrahydrofuran
T=60°C; Kumada-Corriu coupling reaction; 20 h; Inert atmosphere; chemoselective reaction;
参考文献
Ackermann, Lutz; Potukuchi, Harish K.; Kapdi, Anant R.; Schulzke, Carola
Chemistry - A European Journal, 2010 , vol. 16, # 11 p. 3300 - 3303
