1: With potassium hexamethylsilazane in tetrahydrofuran; toluene
T=-78°C; 0.5 h; Inert atmosphere;
2: With oxygen in tetrahydrofuran; toluene
T=-78°C;
3: With hydrogenchloride in tetrahydrofuran; water; toluene
T=20°C; pH=1.2;
参考文献
Bonaparte, Amy C.; Betush, Matthew P.; Panseri, Bettina M.; Mastarone, Daniel J.; Murphy, Ryan K.; Murphree, S. Shaun
Organic Letters, 2011 , vol. 13, # 6 p. 1447 - 1449
