2,4,6-三溴甲基三甲基苯合成路线 （共 8 条）
反应条件
hydrogen bromide; acetic acid T=95°C; 12 h;
参考文献
Made, A. W. van der; Made, R. H. van der
Journal of Organic Chemistry, 1993 , vol. 58, # 5 p. 1262 - 1263
反应条件
formaldehyd; hydrogen bromide in acetic acid
参考文献
Periyasami, Govindasami; Rajesh, Raju; Arumugam, Natarajan; Raghunathan, Raghavachary; Ganesan, Shanmugam; Maruthamuthu, Picha
Journal of Materials Chemistry A, 2013 , vol. 1, # 46 p. 14666 - 14674
反应条件
bromine in various solvent(s) 24 h; Heating;
参考文献
Zavada; Pankova; Holy; Tichy
Synthesis, 1994 , # 11 p. 1132 - 1132
参考文献
Zavada,J. et al.
Collection of Czechoslovak Chemical Communications, 1976 , vol. 41, p. 1777 - 1790
反应条件
in dimethyl sulfoxide T=20°C; 24 h;
参考文献
Podlaha, Jaroslav; Cisarova, Ivana; Alexander, Daniel; Holy, Petr; Kraus, Tomas; Zavada, Jiri
Collection of Czechoslovak Chemical Communications, 2000 , vol. 65, # 10 p. 1587 - 1596
反应条件
in dimethyl sulfoxide T=40°C; 20 h;
参考文献
Zhang, Jianyong; Miller, Philip W.; Nieuwenhuyzen, Mark; James, Stuart L.
Chemistry - A European Journal, 2006 , vol. 12, # 9 p. 2448 - 2453
反应条件
2-Nitropropane; sodium hydride in N,N-dimethyl-formamide T=20°C; 3 h;
参考文献
Balamurugan, Ramalingam; Mohanakrishnan, Arasambattu K.
Tetrahedron, 2007 , vol. 63, # 45 p. 11078 - 11085
反应条件
1: 84 percent / dimethylsulfoxide / 24 h / 20 °C
2: 80 percent / aq. NaOH / ethanol / 14 h / Heating
View Scheme
参考文献
Podlaha, Jaroslav; Cisarova, Ivana; Alexander, Daniel; Holy, Petr; Kraus, Tomas; Zavada, Jiri
Collection of Czechoslovak Chemical Communications, 2000 , vol. 65, # 10 p. 1587 - 1596
