(S)-(+)-1-(Alpha-氨基苄基)-2-萘酚合成路线 (共 8 条)
反应条件
1: With L-(+)-tartaric acid in acetone T=25°C; 6 h; Resolution of racemate; 2: With sodium carbonate in dichloromethane; water Resolution of racemate;
参考文献
Periasamy, Mariappan; Anwar, Shaik; Reddy, Meda Narsi
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2009 , vol. 48, # 9 p. 1261 - 1273
反应条件
sodium carbonate in water 0.5 h;
参考文献
Bian, Guangling; Yang, Shiwei; Huang, Huayin; Song, Ling
Synthesis (Germany), 2013 , vol. 45, # 7 art. no. SS-2012-H0910-OP, p. 899 - 902
反应条件
1: ammonia / ethanol / 20 °C 2: hydrogenchloride / water 3: sodium hydroxide 4: sodium carbonate; L-(+)-tartaric acid / water View Scheme
参考文献
Synthesis (Germany), , vol. 45, # 7 art. no. SS-2012-H0910-OP, p. 899 - 902
反应条件
1: hydrogenchloride / water 2: sodium hydroxide 3: sodium carbonate; L-(+)-tartaric acid / water View Scheme
参考文献
Synthesis (Germany), , vol. 45, # 7 art. no. SS-2012-H0910-OP, p. 899 - 902
反应条件
1: ammonia / ethanol / 20 °C 2: water / dichloromethane / 5 h / 50 °C 3: tetrahydrofuran / 5 h / 20 - 50 °C 4: sodium carbonate / water / 0.5 h View Scheme
参考文献
Synthesis (Germany), , vol. 45, # 7 art. no. SS-2012-H0910-OP, p. 899 - 902
反应条件
1: tetrahydrofuran / 5 h / 20 - 50 °C 2: sodium carbonate / water / 0.5 h View Scheme
参考文献
Synthesis (Germany), , vol. 45, # 7 art. no. SS-2012-H0910-OP, p. 899 - 902
反应条件
1: water / dichloromethane / 5 h / 50 °C 2: tetrahydrofuran / 5 h / 20 - 50 °C 3: sodium carbonate / water / 0.5 h View Scheme
参考文献
Synthesis (Germany), , vol. 45, # 7 art. no. SS-2012-H0910-OP, p. 899 - 902
反应条件
1: 99 percent / methanol / 0.5 h / 20 °C 2: 99 percent / methanol / 0.5 h / 20 °C 3: 95 percent / LiAlH4 / tetrahydrofuran / 0.5 h / Heating View Scheme
参考文献
Dong, Yanmei; Sun, Jianwei; Wang, Xinyan; Xu, Xuenong; Cao, Liya; Hu, Yuefei
Tetrahedron Asymmetry, 2004 , vol. 15, # 10 p. 1667 - 1672