3,4,5-三甲基吡咯-2-甲基乙酯合成路线 （共 37 条）
参考文献
Justus Liebigs Annalen der Chemie, , vol. 517, p. 152,160
反应条件
zinc; sodium nitrite 1.a) glacial acetic acid, H2O, max. 14 deg C, 4 h, b) to r.t., overnight 2.) 1 h, heating; Yield given. Multistep reaction;
参考文献
Chemische Berichte, , vol. 125, # 2 p. 447 - 452
反应条件
sodium hydride 1.) THF, paraffin oil, 1 h, 2.) r.t., 15 min, then reflux, 1 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Journal of Heterocyclic Chemistry, , vol. 28, # 4 p. 939 - 944
参考文献
Curulli, Antonella; Giardi, Maria Teresa; Sleiter, Giancarlo
Gazzetta Chimica Italiana, 1983 , vol. 113, # 1/2 p. 115 - 122
反应条件
T=150 - 160°C; P=73550.8 Torr; Hydrogenation;
参考文献
Chemische Berichte, , vol. 90, p. 87,92
反应条件
1: SO2Cl2; diethyl ether / Erwaermen des Reaktionsprodukts mit H2O 2: aqueous KOH-solution 3: hydrogen chloride; diethyl ether 4: water; NaOH-solution 5: acetic acid; bromine View Scheme
参考文献
Fischer; Hoefelmann
Justus Liebigs Annalen der Chemie, 1938 , vol. 533, p. 216,229
反应条件
1: SO2Cl2; diethyl ether / Erwaermen des Reaktionsprodukts mit H2O 2: aqueous KOH-solution 3: hydrogen chloride; diethyl ether 4: water; NaOH-solution View Scheme
参考文献
Fischer; Hoefelmann
Justus Liebigs Annalen der Chemie, 1938 , vol. 533, p. 216,229
反应条件
1: 65 percent / KOH / ethane-1,2-diol / 5 h / Heating 2: 73 percent / POCl3 / 2 h / 20 °C View Scheme
参考文献
Berezin, M. V.; Semeikin, A. S.; V'yugin, A. I.; Krestov, G. A.
Russian Chemical Bulletin, 1993 , vol. 42, # 3 p. 449 - 453
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1993 , # 3 p. 495 - 499
反应条件
sodium hydroxide; benzoyl chloride 1.) ethylene glycol, reflux 45 min, 2.) toluene, -5-0 deg C, 1 h; Yield givenMultistep reaction;
参考文献
Lash, Timothy D.; Mani, Ukti N.; Drinan, Martin A.; Zhen, Chun; Hall, Troii; Jones, Marjorie A.
Journal of Organic Chemistry, 1999 , vol. 64, # 2 p. 464 - 477
反应条件
1: SO2Cl2; diethyl ether / Erwaermen des Reaktionsprodukts mit H2O 2: 220 °C 3: methanol. NaOH View Scheme
参考文献
Fischer; Hoefelmann
Justus Liebigs Annalen der Chemie, 1938 , vol. 533, p. 216,229
