ANG 453; N-[(5S)-6,7-二氢-9,10,11-三甲氧基-3-(磷酰氧基)-5H-二苯并[a,c]环庚烯-5-基]乙酰胺合成路线 （共 2 条）
反应条件
1: With copper diacetate; zinc in acetic acid T=100°C; 0.416667 h; 2: With acetylacetone in DMF (N,N-dimethyl-formamide) T=55°C; 1 h; 3: With Dowex 50WX8 resin in water; acetonitrile 0.166667 h;
参考文献
AVENTIS PHARMA S.A.
Patent: US2004/138182 A1, 2004 ;
Location in patent: Page 5 ;
反应条件
triethylamine; trichlorophosphate in tetrahydrofuran
参考文献
Broady, Simon D.; Golden, Michael D.; Leonard, John; Muir, James C.; Maudet, Mickael
Tetrahedron Letters, 2007 , vol. 48, # 26 p. 4627 - 4630
