(S)-N-芴甲氧羰基-3-氨基-5-苯基戊酸合成路线 （共 4 条）
反应条件
sodium carbonate in acetone 2 h;
参考文献
Abele, Stefan; Guichard, Gilles; Seebach, Dieter
Helvetica Chimica Acta, 1998 , vol. 81, # 12 p. 2141 - 2156
反应条件
1: 1.) i-BuOCOCl, N-methylmorpholine / 1.) THF, -20 deg C, 20 min; 2.) THF, Et2O, -5 deg C to RT, 4 h 2: 66 percent / H2O, CF3COOAg / tetrahydrofuran; triethylamine / -25 deg C to RT, 4-5 h 3: 440 mg / 1 h / Ambient temperature 4: 64 percent / aq. Na2CO3 / acetone / 2 h View Scheme
参考文献
Helvetica Chimica Acta, , vol. 81, # 12 p. 2141 - 2156
反应条件
1: 440 mg / 1 h / Ambient temperature 2: 64 percent / aq. Na2CO3 / acetone / 2 h View Scheme
参考文献
Helvetica Chimica Acta, , vol. 81, # 12 p. 2141 - 2156
反应条件
1: 66 percent / H2O, CF3COOAg / tetrahydrofuran; triethylamine / -25 deg C to RT, 4-5 h 2: 440 mg / 1 h / Ambient temperature 3: 64 percent / aq. Na2CO3 / acetone / 2 h View Scheme
参考文献
Helvetica Chimica Acta, , vol. 81, # 12 p. 2141 - 2156
