2-(甲氧基甲基)苯甲醚合成路线 (共 16 条)
反应条件
1: 69 percent / sodium borohydride, alkali / methanol
2: potassium carbonate / benzene / Heating
View Scheme
参考文献
Kiong, Lam Soot; Tyman, John H. P.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 1942 - 1952
反应条件
1: thionyl chloride, pyridine / light petroleum
2: 75 percent / t-butyl alcohol, lithium aluminium hydride / bis-(2-methoxy-ethyl) ether / 1 h / -75 °C
3: 69 percent / sodium borohydride, alkali / methanol
4: potassium carbonate / benzene / Heating
View Scheme
参考文献
Kiong, Lam Soot; Tyman, John H. P.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 1942 - 1952
反应条件
1: 75 percent / t-butyl alcohol, lithium aluminium hydride / bis-(2-methoxy-ethyl) ether / 1 h / -75 °C
2: 69 percent / sodium borohydride, alkali / methanol
3: potassium carbonate / benzene / Heating
View Scheme
参考文献
Kiong, Lam Soot; Tyman, John H. P.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 1942 - 1952
反应条件
potassium carbonate in benzene
Heating;
参考文献
Kiong, Lam Soot; Tyman, John H. P.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 1942 - 1952
反应条件
aluminum oxide; potassium hydroxide
3 h; microwave irradiation;
参考文献
Heravi, Majid M.; Ahari, Neda Zamani; Oskooie, Hossein A.; Ghassemzadeh, Mitra
Phosphorus, Sulfur and Silicon and the Related Elements, 2005 , vol. 180, # 7 p. 1701 - 1712
反应条件
potassium hydride
1.) THF, 21 h, 2.) THF, 1 h; Yield given. Multistep reaction;
参考文献
Davies; Goodfellow; Sutton
Tetrahedron Asymmetry, 1992 , vol. 3, # 10 p. 1303 - 1316