4-苯基-2,6,7-三氧杂-1-磷杂双环[2.2.2]辛烷 1-氧化物合成路线 （共 5 条）
反应条件
dinitrogen tetraoxide in chloroform T=0°C;
参考文献
Cooper; Lawston; Rickard; Inch
European Journal of Medicinal Chemistry, 1978 , vol. 13, # 3 p. 207 - 212
反应条件
1: H2 / Pd-C / ethanol / 760 Torr / Ambient temperature 2: P(OEt)3 3: N2O4 / CHCl3 / 0 °C View Scheme
参考文献
Cooper; Lawston; Rickard; Inch
European Journal of Medicinal Chemistry, 1978 , vol. 13, # 3 p. 207 - 212
反应条件
1: LiAlH4 / diethyl ether / 2 h / Heating 2: H2 / Pd-C / ethanol / 760 Torr / Ambient temperature 3: P(OEt)3 4: N2O4 / CHCl3 / 0 °C View Scheme
参考文献
Cooper; Lawston; Rickard; Inch
European Journal of Medicinal Chemistry, 1978 , vol. 13, # 3 p. 207 - 212
反应条件
1: (i) Na, dioxane, (ii) /BRN= 1364034/ 2: LiAlH4 / diethyl ether / 2 h / Heating 3: H2 / Pd-C / ethanol / 760 Torr / Ambient temperature 4: P(OEt)3 5: N2O4 / CHCl3 / 0 °C View Scheme
参考文献
Cooper; Lawston; Rickard; Inch
European Journal of Medicinal Chemistry, 1978 , vol. 13, # 3 p. 207 - 212
反应条件
pyridine; trichlorophosphate in diethyl ether
参考文献
Cooper; Lawston; Rickard; Inch
European Journal of Medicinal Chemistry, 1978 , vol. 13, # 3 p. 207 - 212
