(苯基甲基)氨基甲酸苯酯合成路线 （共 15 条）
反应条件
triethylsilane; trifluoroacetic acid in acetonitrile
T=22°C; 18 h;
参考文献
Dube, Daniel; Scholte, Andrew A.
Tetrahedron Letters, 1999 , vol. 40, # 12 p. 2295 - 2298
反应条件
triethylsilane; 1,1,1,3,3,3-hexamethyl-disilazane; iron(II) sulfate in dichloromethane
T=20°C; 24 h;
参考文献
Yang, Bai-Ling; Tian, Shi-Kai
European Journal of Organic Chemistry, 2007 , # 28 p. 4646 - 4650
反应条件
samarium diiodide in tetrahydrofuran
T=20°C; Reduction; 0.333333 h;
参考文献
Keck, Gary E.; Wager, Travis T.; McHardy, Stanton F.
Tetrahedron, 1999 , vol. 55, # 40 p. 11755 - 11772
反应条件
1: N-benzyl O-methyl thiocarbamate With pyridine; bis(trichloromethyl) carbonate in dichloromethane
T=-10°C;
2: phenol in dichloromethane
T=-10 - 30°C; 14 h;
参考文献
Joshi, Uday M.; Patkar, Laxmikant N.; Rajappa, Srinivasachari
Synthetic Communications, 2004 , vol. 34, # 1 p. 33 - 39
参考文献
Kolbezen et al.
Journal of Agricultural and Food Chemistry, 1954 , vol. 2, p. 864,865, 866
反应条件
1: bis(trichloromethyl) carbonate With pyridine; resin-nitrophenol in dichloromethane
T=20°C; 2 h;
2: phenol With pyridine; 4-(N,N-dimethlyamino)pyridine in dichloromethane
T=20°C; 2.5 h;
3: benzylamine in dichloromethane
T=20°C; 20 h; Further stages.;
参考文献
Mormeneo, David; Llebaria, Amadeu; Delgado, Antonio
Tetrahedron Letters, 2004 , vol. 45, # 37 p. 6831 - 6834
参考文献
Bridgeman, Eve; Tomkinson, Nicholas C. O.
Synlett, 2006 , # 2 p. 243 - 246
反应条件
in benzene
a.) RT, 1 h, b.) reflux, 1 h;
参考文献
Patonay, Tamas; Patonay-Peli, Erzsebet; Mogyorodi, Ferenc
Synthetic Communications, 1990 , vol. 20, # 18 p. 2865 - 2885
反应条件
1: DMAP / CH2Cl2; pyridine / 16 h
2: 48 percent / SmI2 / tetrahydrofuran / 0.33 h / 20 °C
View Scheme
参考文献
Keck, Gary E.; Wager, Travis T.; McHardy, Stanton F.
Tetrahedron, 1999 , vol. 55, # 40 p. 11755 - 11772
反应条件
1: 90 percent / pyridine / 17 h
2: 70 percent / NaCNBH3; 2N HCl / CH2Cl2; methanol / 20 h / pH 3
3: DMAP / CH2Cl2; pyridine / 16 h
4: 48 percent / SmI2 / tetrahydrofuran / 0.33 h / 20 °C
View Scheme
参考文献
Keck, Gary E.; Wager, Travis T.; McHardy, Stanton F.
Tetrahedron, 1999 , vol. 55, # 40 p. 11755 - 11772
