(苯基甲基)氨基甲酸苯酯合成路线 （共 15 条）
反应条件
1: DMAP / CH2Cl2; pyridine / 16 h
2: 48 percent / SmI2 / tetrahydrofuran / 0.33 h / 20 °C
View Scheme
参考文献
Keck, Gary E.; Wager, Travis T.; McHardy, Stanton F.
Tetrahedron, 1999 , vol. 55, # 40 p. 11755 - 11772
反应条件
1: 70 percent / NaCNBH3; 2N HCl / CH2Cl2; methanol / 20 h / pH 3
2: DMAP / CH2Cl2; pyridine / 16 h
3: 48 percent / SmI2 / tetrahydrofuran / 0.33 h / 20 °C
View Scheme
参考文献
Keck, Gary E.; Wager, Travis T.; McHardy, Stanton F.
Tetrahedron, 1999 , vol. 55, # 40 p. 11755 - 11772
反应条件
1: 88.6 percent / Et3N / CH2Cl2 / 1.67 h / 5 °C
2: 56.8 percent / benzene / a.) RT, 1 h, b.) reflux, 1 h
View Scheme
参考文献
Patonay, Tamas; Patonay-Peli, Erzsebet; Mogyorodi, Ferenc
Synthetic Communications, 1990 , vol. 20, # 18 p. 2865 - 2885
反应条件
dimethyl sulfoxide in water; acetonitrile
T=25°C; Kinetics;
参考文献
Um, Ik-Hwan; Kim, Eun Young; Park, Hye-Ran; Jeon, Sang-Eun
Journal of Organic Chemistry, 2006 , vol. 71, # 6 p. 2302 - 2306
反应条件
in methanol
0.25 h; microwave irradiation;
参考文献
Bridgeman, Eve; Tomkinson, Nicholas C. O.
Synlett, 2006 , # 2 p. 243 - 246
