N,N-二苄基-1-丁胺合成路线 （共 20 条）
反应条件
palladium diacetate; triphenylphosphine in tetrahydrofuran
T=110°C; P=15514.9 Torr; 15 h;
参考文献
Troisi, Luigino; Granito, Catia; Rosato, Francesca; Videtta, Valeria
Tetrahedron Letters, 2010 , vol. 51, # 2 p. 371 - 373
反应条件
1.1: 90 percent / aq. CAN / acetonitrile / 20 °C
2.1: HC(OMe)3 / methanol / 20 °C / pH 6
2.2: 76 percent / NaBH4 / methanol / 16 h / 0 °C
View Scheme
参考文献
Bull, Steven D.; Davies, Stephen G.; Fenton, Carry; Mulvaney, Andrew W.; Shyam Prasad; Smith, Andrew D.
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 22 p. 3765 - 3774
反应条件
1: 69 percent / 4 Angstroem molecular sieves / diethyl ether / 12 h / 20 °C
2: 27 percent Chromat. / SmI2 / tetrahydrofuran; hexamethylphosphoric acid triamide / 0 - 20 °C
View Scheme
参考文献
Katritzky, Alan R.; Luo, Zhushou; Fang, Yunfeng; Feng, Daming; Ghiviriga, Ion
Journal of the Chemical Society. Perkin Transactions 2, 2000 , # 7 p. 1375 - 1380
反应条件
1: 69 percent / 4 Angstroem molecular sieves / diethyl ether / 12 h / 20 °C
2: 27 percent Chromat. / SmI2 / tetrahydrofuran; hexamethylphosphoric acid triamide / 0 - 20 °C
View Scheme
参考文献
Katritzky, Alan R.; Luo, Zhushou; Fang, Yunfeng; Feng, Daming; Ghiviriga, Ion
Journal of the Chemical Society. Perkin Transactions 2, 2000 , # 7 p. 1375 - 1380
反应条件
oxygen
Et2O, 1) -20 deg C / 2h 2) -20 deg C; Yield given. Multistep reaction;
参考文献
Yamamoto, Hisashi; Maruoka, Keiji
Journal of Organic Chemistry, 1980 , vol. 45, # 13 p. 2739 - 2740
反应条件
sodium hydrogencarbonate
参考文献
Labriola; Dorronsoro; Verruno
Anales de la Asociacion Quimica Argentina (1921-2001), 1949 , vol. 37, p. 79,84
反应条件
lithium aluminium tetrahydride; tungsten hexachloride in chlorobenzene
5 h; Ambient temperature; Product distributionMechanism;
参考文献
Ikariya, Takao; Ishikawa, Yasutoshi; Hirai, Kiyomiki; Yoshikawa, Sadao
Journal of Organometallic Chemistry, 1985 , vol. 288, p. 311 - 316
反应条件
lithium aluminium tetrahydride; tungsten hexachloride; triphenylphosphine in chlorobenzene
20 h; Ambient temperaturedifferent molar ratio of PPh3; Product distribution;
参考文献
Ikariya, Takao; Ishikawa, Yasutoshi; Hirai, Kiyomiki; Yoshikawa, Sadao
Journal of Organometallic Chemistry, 1985 , vol. 288, p. 311 - 316
反应条件
N-tert-butyl-N',N'-diethylformamidine
T=55°C; other bases; labeling studies ((13)CO2 and R1R2(15)NH) for other amines; Product distribution;
参考文献
McGhee, William; Riley, Dennis; Christ, Kevin; Pan, Yi; Parnas, Barry
Journal of Organic Chemistry, 1995 , vol. 60, # 9 p. 2820 - 2830
反应条件
in methanol
T=24.84°C; KineticsThermodynamic data; Temperature;
参考文献
Ravi; Sanjeev; Jagannadham
International Journal of Chemical Kinetics, 2013 , vol. 45, # 12 p. 803 - 810
