1: With trimethyl orthoformate in methanol T=20°C; pH=6; 2: With sodium tetrahydroborate in methanol T=0°C; 5 h; Further stages.;
参考文献
Bull, Steven D.; Davies, Stephen G.; Fenton, Carry; Mulvaney, Andrew W.; Shyam Prasad; Smith, Andrew D.
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 22 p. 3765 - 3774
1.1: 90 percent / aq. CAN / acetonitrile / 20 °C 2.1: HC(OMe)3 / methanol / 20 °C / pH 6 2.2: 77 percent / NaBH4 / methanol / 5 h / 0 °C View Scheme
参考文献
Bull, Steven D.; Davies, Stephen G.; Fenton, Carry; Mulvaney, Andrew W.; Shyam Prasad; Smith, Andrew D.
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 22 p. 3765 - 3774
ammonium cerium(IV) nitrate in tetrahydrofuran; acetonitrile
T=20°C;
参考文献
Bull, Steven D.; Davies, Stephen G.; Fenton, Carry; Mulvaney, Andrew W.; Shyam Prasad; Smith, Andrew D.
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 22 p. 3765 - 3774
