(1-甲氧基-3-丁烯)-苯合成路线 (共 60 条)
反应条件
n-butyllithium; (cyclopropyl)2ZrCl2 in tetrahydrofuran T=-78 - 20°C;
参考文献
Gandon, Vincent; Laroche, Christophe; Szymoniak, Jan
Tetrahedron Letters, 2003 , vol. 44, # 26 p. 4827 - 4829
反应条件
trimethylaluminum; aluminum tri-bromide; copper(I) bromide in dichloromethane; toluene
T=20°C; 3 h;
参考文献
Jung, Michael E.; Maderna, Andreas
Tetrahedron Letters, 2004 , vol. 45, # 27 p. 5301 - 5304
反应条件
aluminum tri-bromide; lead(II) bromide; aluminium in tetrahydrofuran
1 h; Ambient temperature;
参考文献
Tanaka,Hideo; Yamashita, Shiro; Ikemoto, Youichi; Torii, Sigeru
Tetrahedron Letters, 1988 , vol. 29, # 14 p. 1721 - 1724
反应条件
1: C18H12F3S3(1+); (methoxy(phenylthio)methyl)benzene With tetra-n-butylammonium tetrafluoroborate in dichloromethane
T=-78°C; 0.166667 h;
2: allyl-trimethyl-silane With tetra-n-butylammonium tetrafluoroborate in dichloromethane
T=-78°C; 1 h;
参考文献
Suga, Seiji; Matsumoto, Kouichi; Ueoka, Koji; Yoshida, Jun-Ichi
Journal of the American Chemical Society, 2006 , vol. 128, # 24 p. 7710 - 7711
反应条件
scandium tris(trifluoromethanesulfonate) in dichloromethane
T=20°C; 5 h;
参考文献
Yadav, Jhillu S.; Subba Reddy, Basi V.; Srihari
Synlett, 2001 , # 5 p. 673 - 675
反应条件
trimethylsilyl trifluoromethanesulfonate in tetrahydrofuran
T=-78 - 0°C;
参考文献
Hunter, Roger; Michael, Joseph P.; Tomlinson, Geoffrey D.
Tetrahedron, 1994 , vol. 50, # 3 p. 871 - 888
反应条件
1: (methoxy(phenylthio)methyl)benzene With C18H12F3S3(1+); tetra-n-butylammonium tetrafluoroborate in dichloromethane
T=-78°C; 0.166667 h; Electrochemical reactionInert atmosphere;
2: allyl-trimethyl-silane in dichloromethane
T=-78°C; 1 h; Inert atmosphere;
参考文献
Matsumoto, Kouichi; Ueoka, Koji; Suzuki, Shinkiti; Suga, Seiji; Yoshida, Jun-ichi
Tetrahedron, 2009 , vol. 65, # 52 p. 10901 - 10907
反应条件
iodine in dichloromethane
T=40°C; 1 h;
参考文献
Sakurai, Hideki; Sasaki, Koshi; Hayashi, Josaburo; Hosomi, Akira
Journal of Organic Chemistry, 1984 , vol. 49, # 15 p. 2808 - 2809
反应条件
platinum (II) chloride in acetonitrile
T=20°C; Substitution; Allylation; 12 h;
参考文献
Fuerstner, Alois; Voigtlaender, David
Synthesis, 2000 , # 7 p. 959 - 969
反应条件
indium(III) chloride in dichloromethane
T=20°C; 3 h;
参考文献
Merisor, Elena; Conrad, Juergen; Malakar, Chandi C.; Beifuss, Uwe
Synlett, 2008 , # 6 p. 903 - 907