(1-甲氧基-3-丁烯)-苯合成路线 (共 60 条)
反应条件
Al-MCM-41 in dichloromethane
T=30°C; Sakurai allylation; 0.75 h; Inert atmosphere;
参考文献
Ito, Suguru; Hayashi, Akira; Komai, Hirotomo; Kubota, Yoshihiro; Asami, Masatoshi
Tetrahedron Letters, 2010 , vol. 51, # 32 p. 4243 - 4245
反应条件
titanium tetrachloride in dichloromethane
T=-78°C; 1 h;
参考文献
Dussault; Lee, In Quen; Lee; Niu; Schultz; Zope
Journal of Organic Chemistry, 2000 , vol. 65, # 25 p. 8407 - 8414
反应条件
35 percent H3PW12O40 modified aluminium-incorporated mesoporous KIT-6 in acetonitrile
T=20°C; Hosomi-Sakurai Reaction; 2 h; Green chemistry;
参考文献
Fazaeli, Razieh; Aliyan, Hamid; Naderi, Elham
Phosphorus, Sulfur and Silicon and the Related Elements, 2013 , vol. 188, # 6 p. 745 - 754
反应条件
trimethylsilyl iodide in dichloromethane
T=-78°C; 1 h;
参考文献
Sakurai, Hideki; Sasaki, Koshi; Hosomi, Akira
Tetrahedron Letters, 1981 , vol. 22, p. 745 - 748
反应条件
acetyl chloride; zinc(II) chloride in dichloromethane
2 h; Ambient temperature; Yields of byproduct given;
参考文献
Oriyama, Takeshi; Iwanami, Katsuyuki; Tsukamoto, Kazuhisa; Ichimura, Yuichi; Koga, Gen
Bulletin of the Chemical Society of Japan, 1991 , vol. 64, # 4 p. 1410 - 1412
反应条件
zinc(II) chloride in dichloromethane
T=-78°C; 15 h;
参考文献
Dau-Schmidt, Jan-Peter; Mayr, Herbert
Chemische Berichte, 1994 , vol. 127, # 1 p. 205 - 212
反应条件
4 A molecular sieve; tetra-n-butylammonium perchlorate in dichloromethane
T=20°C; Alkylation; Electrochemical reaction;
参考文献
Yoshida, Jun-Ichi; Sugawara, Masanobu; Tatsumi, Masao; Rise, Naoki
Journal of Organic Chemistry, 1998 , vol. 63, # 17 p. 5950 - 5961
反应条件
allyl bromide; aluminium; aluminum tri-bromide; lead(II) bromide in tetrahydrofuran
0.25 h; Ambient temperature;
参考文献
Tanaka,Hideo; Yamashita, Shiro; Ikemoto, Youichi; Torii, Sigeru
Tetrahedron Letters, 1988 , vol. 29, # 14 p. 1721 - 1724
反应条件
(i) NaH, (ii) /BRN= 969135/; Multistep reaction;
参考文献
Baldry,P.J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1975 , p. 1913 - 1920
反应条件
titanium tetrachloride in dichloromethane
T=-78°C; 1 h;
参考文献
Hermans, Bernard; Hevesi, Laszlo
Journal of Organic Chemistry, 1995 , vol. 60, # 19 p. 6141 - 6147