(1-甲氧基-3-丁烯)-苯合成路线 （共 60 条）
反应条件
allyltributylstannane; titanium tetrachloride in dichloromethane
T=-78°C; 1 h;
参考文献
Hermans, Bernard; Hevesi, Laszlo
Journal of Organic Chemistry, 1995 , vol. 60, # 19 p. 6141 - 6147
反应条件
InOTf in toluene
T=25°C; 16 h; Inert atmosphere;
参考文献
Schneider, Uwe; Dao, Hai T.; Kobayashi, Shu
Organic Letters, 2010 , vol. 12, # 11 p. 2488 - 2491
反应条件
in diethyl ether; toluene
T=25°C; 1.5 h;
参考文献
Baruah, Mukulesh; Bols, Mikael
Journal of the Chemical Society. Perkin Transactions 1, 2002 , # 4 p. 509 - 512
反应条件
trimethylsilyl trifluoromethanesulfonate in tetrahydrofuran
T=-78 - 0°C;
参考文献
Hunter, Roger; Michael, Joseph P.; Tomlinson, Geoffrey D.
Tetrahedron, 1994 , vol. 50, # 3 p. 871 - 888
反应条件
titanium tetrachloride in dichloromethane
T=-78°C; 1 h;
参考文献
Hermans, Bernard; Hevesi, Laszlo
Journal of Organic Chemistry, 1995 , vol. 60, # 19 p. 6141 - 6147
反应条件
1: Bi(OTf)3*xH2O / acetonitrile
2: 22 percent / KBr / Ni(1,4,8,11-tetraazacyclotetradecane)Br2 / dimethylformamide / 25 °C / Electrochemical reaction
View Scheme
参考文献
Olivero, Sandra; Perriot, Rodolphe; Dunach, Elisabet; Baru, Ashvin R.; Bell, Eric D.; Mohan, Ram S.
Synlett, 2006 , # 13 p. 2021 - 2026
反应条件
1: 88 percent / Bi(OTf)3*xH2O / CH2Cl2
2: 22 percent / KBr / Ni(tmc)Br2 / dimethylformamide / 25 °C / Electrochemical reaction
View Scheme
参考文献
Olivero, Sandra; Perriot, Rodolphe; Dunach, Elisabet; Baru, Ashvin R.; Bell, Eric D.; Mohan, Ram S.
Synlett, 2006 , # 13 p. 2021 - 2026
反应条件
1: Bi(OTf)3*xH2O / methanol
2: Bi(OTf)3*xH2O / acetonitrile
3: 22 percent / KBr / Ni(1,4,8,11-tetraazacyclotetradecane)Br2 / dimethylformamide / 25 °C / Electrochemical reaction
View Scheme
参考文献
Olivero, Sandra; Perriot, Rodolphe; Dunach, Elisabet; Baru, Ashvin R.; Bell, Eric D.; Mohan, Ram S.
Synlett, 2006 , # 13 p. 2021 - 2026
反应条件
boron trifluoride diethyl etherate in tetrahydrofuran
T=-20°C; 2 h; Yield given. Yields of byproduct given;
参考文献
Sato, Tsuneo; Okura, Shuji; Otera, Junzo; Nozaki, Hitosi
Tetrahedron Letters, 1987 , vol. 28, # 50 p. 6299 - 6302
反应条件
Al-MCM-41 in dichloromethane
T=30°C; Sakurai allylation; 0.75 h; Inert atmosphere;
参考文献
Ito, Suguru; Hayashi, Akira; Komai, Hirotomo; Kubota, Yoshihiro; Asami, Masatoshi
Tetrahedron Letters, 2010 , vol. 51, # 32 p. 4243 - 4245
