(1-甲氧基-3-丁烯)-苯合成路线 （共 60 条）
反应条件
Al-MCM-41 (Si/Al = 26) in dichloromethane
T=30°C; 0.75 h;
参考文献
Ito, Suguru; Hayashi, Akira; Komai, Hirotomo; Yamaguchi, Hitoshi; Kubota, Yoshihiro; Asami, Masatoshi
Tetrahedron, 2011 , vol. 67, # 11 p. 2081 - 2089
反应条件
tetraethylammonium p-toluenesulfonate
electrolysis, undivided cell, carbon rod electrodes;
参考文献
Yoshida, Jun-ichi; Murata, Toshiki; Isoe, Sachihiko
Tetrahedron Letters, 1986 , vol. 27, # 29 p. 3373 - 3376
参考文献
Okajima, Masayuki; Suga, Seiji; Itami, Kenichiro; Yoshida, Jun-Ichi
Journal of the American Chemical Society, 2005 , vol. 127, # 19 p. 6930 - 6931
反应条件
1: O3; O2 / methanol; CH2Cl2 / -78 °C
2: imidazole / CH2Cl2; dimethylformamide
3: 69 percent / TiCl4 / CH2Cl2 / 1 h / -78 °C
View Scheme
参考文献
Dussault; Lee, In Quen; Lee; Niu; Schultz; Zope
Journal of Organic Chemistry, 2000 , vol. 65, # 25 p. 8407 - 8414
反应条件
1: imidazole / CH2Cl2; dimethylformamide
2: 69 percent / TiCl4 / CH2Cl2 / 1 h / -78 °C
View Scheme
参考文献
Dussault; Lee, In Quen; Lee; Niu; Schultz; Zope
Journal of Organic Chemistry, 2000 , vol. 65, # 25 p. 8407 - 8414
反应条件
1.1: tetrahydrofuran / 0.17 h / 0 °C
1.2: 68 percent / tetrahydrofuran / 1 h / 0 °C
2.1: O3; O2 / methanol; CH2Cl2 / -78 °C
3.1: imidazole / CH2Cl2; dimethylformamide
4.1: 69 percent / TiCl4 / CH2Cl2 / 1 h / -78 °C
View Scheme
参考文献
Dussault; Lee, In Quen; Lee; Niu; Schultz; Zope
Journal of Organic Chemistry, 2000 , vol. 65, # 25 p. 8407 - 8414
反应条件
1: 67 percent / BF3*OEt2 / toluene; hexane / 8 h / -78 °C
2: 47 percent / molecular sieves 4 Angstroem; Bu4NClO4 / CH2Cl2 / 20 °C / Electrochemical reaction
View Scheme
参考文献
Yoshida, Jun-Ichi; Sugawara, Masanobu; Tatsumi, Masao; Rise, Naoki
Journal of Organic Chemistry, 1998 , vol. 63, # 17 p. 5950 - 5961
反应条件
1: 1.) NaH, 2.) n-BuLi / 1.) DMF, room temp., overnight, 2.) THF, hexane, -78 deg C, 20 min
2: n-Bu3SnH, Et3B, AIBN / toluene / -20 °C / other temp., other solvent, various molar ratio
View Scheme
参考文献
Rawal; Singh; Dufour; Michoud
Journal of Organic Chemistry, 1993 , vol. 58, # 27 p. 7718 - 7727
反应条件
aluminium; aluminum tri-bromide; lead(II) bromide in tetrahydrofuran
0.25 h; Product distribution;
参考文献
Tanaka,Hideo; Yamashita, Shiro; Ikemoto, Youichi; Torii, Sigeru
Tetrahedron Letters, 1988 , vol. 29, # 14 p. 1721 - 1724
反应条件
1: BuLi (1.1 eq.), CuI (0.5 eq.) / tetrahydrofuran / 3 h / -78 °C
2: (2. eq.) BF3OEt2 / tetrahydrofuran / 2 h / -20 °C
View Scheme
参考文献
Sato, Tsuneo; Okura, Shuji; Otera, Junzo; Nozaki, Hitosi
Tetrahedron Letters, 1987 , vol. 28, # 50 p. 6299 - 6302
