1-(苄基磺酰基)-2-硝基苯合成路线 （共 9 条）
反应条件
1: phenylmethanethiol With sodium in methanol T=20°C; 2: 1-chloro-2-nitro-benzene in methanol Reflux;
参考文献
Li, Zai-Shun; Wang, Wei-Min; Lu, Wei; Niu, Cong-Wei; Li, Yong-Hong; Li, Zheng-Ming; Wang, Jian-Guo
Bioorganic and Medicinal Chemistry Letters, 2013 , vol. 23, # 13 p. 3723 - 3727
反应条件
Pd(2-[2-(benzylthio)phenyliminomethyl]-4-bromophenol-(H))Cl; potassium carbonate in N,N-dimethyl-formamide T=90°C; 5 h; Sealed tubeInert atmosphere;
参考文献
Gogoi, Prasanta; Kalita, Mukul; Barman, Pranjit
Synlett, 2014 , vol. 25, # 6 art. no. 47, p. 866 - 870
反应条件
Cu(I) 3-methylsalicylate; sodium L-ascorbate in water T=70°C; 168 h; Inert atmosphere;
参考文献
Martinek, Marek; Korf, Michal; Srogl, Jiri
Chemical Communications, 2010 , vol. 46, # 24 p. 4387 - 4389
反应条件
sodium hydroxide in ethanol 1.) 15 min 2.) reflux, 14 h;
参考文献
Courtin, Alfred; Tobel, Hans-Rudolf von; Auerbach, Guenther
Helvetica Chimica Acta, 1980 , vol. 63, # 6 p. 1412 - 1419
反应条件
potassium carbonate in ethanol T=90°C; 0.166667 h; Microwave irradiation;
参考文献
Chemistry - An Asian Journal, , vol. 7, # 1 p. 45 - 49
反应条件
1: in ethanol 6 h; Reflux; 2: With sodium hydroxide in ethanol 2 h; Reflux;
参考文献
Synlett, , vol. 24, # 7 art. no. ST-2012-D0136-L, p. 873 - 877
反应条件
thionyl chloride in chloroform T=45°C; 1 h;
参考文献
Li, Zai-Shun; Wang, Wei-Min; Lu, Wei; Niu, Cong-Wei; Li, Yong-Hong; Li, Zheng-Ming; Wang, Jian-Guo
Bioorganic and Medicinal Chemistry Letters, 2013 , vol. 23, # 13 p. 3723 - 3727
反应条件
1: sulfuryl dichloride / 1,2-dichloro-ethane
2: triethylamine / N,N-dimethyl-formamide / 0.5 h / 20 °C
View Scheme
参考文献
Shang, Jian-Li; Guo, Hui; Li, Zai-Shun; Ren, Biao; Li, Zheng-Ming; Dai, Huan-Qin; Zhang, Li-Xin; Wang, Jian-Guo
Bioorganic and Medicinal Chemistry Letters, 2013 , vol. 23, # 3 p. 724 - 727
反应条件
ethanol; nickel
Hydrogenation;
参考文献
Sieglitz; Koch
Chemische Berichte, 1925 , vol. 58, p. 79
