1-(3-甲基喹喔啉-2-基)乙酮合成路线 （共 19 条）
反应条件
methanol; potassium borohydride
参考文献
Journal of the Chemical Society, , p. 1423,1428
反应条件
N-bromosuccinmide in water
T=70°C; 4.33333 h;
参考文献
Anil Kumar; Madhav; Harsha Vardhan Reddy; Nageswar
Tetrahedron Letters, 2011 , vol. 52, # 22 p. 2862 - 2865
反应条件
1: in ethanol
0.5 h; Reflux;
2: With sodium dithionite in ethanol
2 h; Reflux;
参考文献
Zhang, Jiaheng; He, Xin; Gao, Haixiang
Journal of Molecular Structure, 2011 , vol. 1004, # 1-3 p. 109 - 115
反应条件
in toluene
T=180°C; 0.05 h; Microwave irradiation;
参考文献
Castillo, Juan-Carlos; Presset, Marc; Abonia, Rodrigo; Coquerel, Yoann; Rodriguez, Jean
European Journal of Organic Chemistry, 2012 , # 12 p. 2338 - 2345
反应条件
1: triethylamine
2: sodium dithionite / methanol; water / 0.17 h / 70 °C
View Scheme
参考文献
Burguete, Asuncion; Pontiki, Eleni; Hadjipavlou-Litina, Dimitra; Ancizu, Saioa; Villar, Raquel; Solano, Beatriz; Moreno, Elsa; Torres, Enrique; Perez, Silvia; Aldana, Ignacio; Monge, Antonio
Chemical Biology and Drug Design, 2011 , vol. 77, # 4 p. 255 - 267
反应条件
1: calcium chloride; aminoethyl alcohol
2: sodium dithionite / methanol; ethyl acetate / 65 °C
View Scheme
参考文献
Gil, Ana; Pabon, Adriana; Galiano, Silvia; Burguete, Asuncion; Perez-Silanes, Silvia; Deharo, Eric; Monge, Antonio; Aldana, Ignacio
Molecules, 2014 , vol. 19, # 2 p. 2166 - 2180
反应条件
acetic acid
T=100°C; 4 h;
参考文献
Budyka, M. F.; Kantor, M. M.; Alfimov, M. V.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1991 , vol. 27, # 10 p. 1072 - 1075
Khimiya Geterotsiklicheskikh Soedinenii, 1991 , vol. 27, # 10 p. 1340 - 1343
反应条件
1: triethylamine
2: sodium dithionite / methanol; water / 0.17 h / 70 °C
View Scheme
参考文献
Burguete, Asuncion; Pontiki, Eleni; Hadjipavlou-Litina, Dimitra; Ancizu, Saioa; Villar, Raquel; Solano, Beatriz; Moreno, Elsa; Torres, Enrique; Perez, Silvia; Aldana, Ignacio; Monge, Antonio
Chemical Biology and Drug Design, 2011 , vol. 77, # 4 p. 255 - 267
参考文献
Sachs; Roehmer
Chemische Berichte, 1902 , vol. 35, p. 3313
Full Text Show Details
Sachs; Barschall
Chemische Berichte, 1901 , vol. 34, p. 3053
反应条件
1: benzene
2: aqueous H2SO4; FeCl3
View Scheme
参考文献
Barltrop et al.
Journal of the Chemical Society, 1959 , p. 1132,1133
