1-环己基-2-甲氧基苯合成路线 （共 29 条）
反应条件
1: hydrobromic acid; glacial acetic acid 2: alcoholic KOH-solution View Scheme
参考文献
Bodroux
Annales de Chimie (Cachan, France), 1929 , vol. <10> 11, p. 519,525
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1928 , vol. 186, p. 1005
反应条件
hydrogen bromide; acetic acid
参考文献
Annales de Chimie (Cachan, France), , vol. <10> 11, p. 519,525
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, , vol. 186, p. 1005
反应条件
1: diethyl ether / anschliessendes Behandeln mit CO2 2: HI View Scheme
参考文献
Burtner; Brown
Journal of the American Chemical Society, 1953 , vol. 75, p. 2334,2337
反应条件
anhydrous iron chloride; N,N,N',N,-tetramethylethylenediamine in tetrahydrofuran
T=0 - 20°C; 4 h; Inert atmosphere;
参考文献
Czaplik, Waldemar Maximilian; Mayer, Matthias; Von Wangelin, Axel Jacobi
Angewandte Chemie - International Edition, 2009 , vol. 48, # 3 p. 607 - 610
反应条件
N,N,N',N,-tetramethylethylenediamine; magnesium; anhydrous iron chloride in tetrahydrofuran
T=0 - 20°C; Inert atmosphere; Product distribution / selectivity;
参考文献
SALTIGO GMBH
Patent: US2009/247764 A1, 2009 ;
Location in patent: Page/Page column 7 ;
反应条件
palladium diacetate; caesium carbonate; di-(1-adamantyl)-n-butylphosphine in water; toluene
T=100°C; Suzuki-Miyaura coupling; 72 h; Inert atmosphere;
参考文献
Dreher, Spencer D.; Dormer, Peter G.; Sandrock, Deidre L.; Molander, Gary A.
Journal of the American Chemical Society, 2008 , vol. 130, # 29 p. 9257 - 9259
反应条件
N,N,N',N,-tetramethylethylenediamine; Co(acac)3 in tetrahydrofuran
T=0°C; 0.666667 h; Inert atmosphere; chemoselective reaction;
参考文献
Cahiez, Gerard; Chaboche, Christophe; Duplais, Christophe; Moyeux, Alban
Organic Letters, 2009 , vol. 11, # 2 p. 277 - 280
反应条件
1: cyclohexyl magnesium bromide With zinc(II) chloride in tetrahydrofuran
T=20°C; 1 h;
2: 1-iodo-2-methoxybenzene With dichloro bis(acetonitrile) palladium(II) in tetrahydrofuran
T=20°C; Negishi coupling; 2 h; Further stages.;
参考文献
Luo, Xiancai; Zhang, Heng; Duan, Hui; Liu, Qiang; Zhu, Lizheng; Zhang, Tony; Lei, Aiwen
Organic Letters, 2007 , vol. 9, # 22 p. 4571 - 4574
参考文献
Lefebvre; Levas
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1945 , vol. 220, p. 826
Full Text Show Details
Levas
Annales de Chimie (Cachan, France), 1948 , vol. <12> 3, p. 145,191
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1946 , vol. 223, p. 901,903 Anm.
反应条件
aluminium trichloride
参考文献
Abdurasulewa
Doklady Akademii Nauk UzSSR, 1957 , # 7 p. 39
Chem.Abstr., 1959 , p. 9113
