反-1,4-二甲基环己烷合成路线 (共 48 条)
反应条件
hydrogen; tetra(n-butyl)ammonium hydrogensulfate; rhodium colloidal catalyst in water T=36°C; Catalytic hydrogenation; P=180014 Torr; pH=7.5; 62 h;
参考文献
Chemical Communications, , # 11 p. 941 - 942
反应条件
[Rh(η3-C3H5)3]; C68H88O6P2; hydrogen in n-heptane T=80°C; P=30003 Torr; 16 h; AutoclaveGlovebox; TemperaturePressure; stereoselective reaction;
参考文献
Catalysis Science and Technology, , vol. 3, # 10 p. 2828 - 2833
反应条件
hydrogen; palladium on activated charcoal
参考文献
Angewandte Chemie, , vol. 92, # 8 p. 651 - 652
反应条件
nickel contacts; hydrogen T=175°C;
参考文献
Journal of Organic Chemistry, , vol. 27, p. 486,488
Chemische Berichte, , vol. 65, p. 1613,1617
Zhurnal Obshchei Khimii, , vol. 2, p. 755,760
反应条件
tri-isobutyl aluminium; palladium dichloride in tetrachloromethane T=8 - 50°C; 2 h; Further byproducts given;
参考文献
Russian Chemical Bulletin, , vol. 50, # 7 p. 1326 - 1329
反应条件
1: Raney nickel; ethanol / Hydrogenation 2: nickel contacts; hydrogen / 175 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 27, p. 486,488
反应条件
tri-n-butyl-tin hydride in benzene T=60°C; 1 h; Irradiationother hydrides; Product distribution;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 23, # 2 p. 291 - 294
Zhurnal Organicheskoi Khimii, , vol. 23, # 2 p. 327 - 331
反应条件
aluminium trichloride T=56°C;
参考文献
Bulletin des Societes Chimiques Belges, , vol. 53, p. 45,47
Bulletin des Societes Chimiques Belges, , vol. 59, p. 140,152
反应条件
mercury T=55°C; 3 h; Irradiationdetermination of kdis/krec; longer reaction times; isomerization product distribution, estimation of cis/trans ratio in the disproportionation; addition of 1,4-dimethylcyclohexene; Kinetics;
参考文献
Journal of the American Chemical Society, , vol. 111, # 8 p. 2935 - 2946
反应条件
tri-isobutyl aluminium; palladium dichloride in tetrachloromethane T=8 - 50°C; 2 h; Further byproducts given;
参考文献
Russian Chemical Bulletin, , vol. 50, # 7 p. 1326 - 1329