3-辛酰基硫代丙基三乙氧基硅烷合成路线 （共 6 条）
反应条件
triethylamine in hexane T=0°C; 2 h;
参考文献
Cruse, Richard W.; York, W. Michael; Pohl, Eric R.; Chaves, Antonio; Simandan, Tiberiu L.; Joshi, Prashant
Patent: US2008/161590 A1, 2008 ;
Location in patent: Page/Page column 11 ;
反应条件
2-(N,N-dimethylamino)-pyridine in toluene T=70°C; 2 h;
参考文献
US2012/296023 A1, ;
Page/Page column 8 ;
反应条件
Aliquatreg; 336 in water T=50 - 74°C; 24 h; Product distribution / selectivity;
参考文献
WO2005/7661 A1, ;
Page/Page column 23-24 ;
反应条件
1: gamma-mercaptopropyltriethoxysilane With sodium in toluene T=105°C; 0.5 - 1.36667 h; 2: octanoic acid chloride in toluene T=20 - 62°C; 1 - 1.58333 h; 3: With water in toluene T=32 - 50°C; Product distribution / selectivity;
参考文献
US6777569 B1, ;
Page column 6 ;
反应条件
1: 4,4,13,13-tetraethoxy-3,14-dioxa-8,9-dithia-4,13-disilahexadecane With sodium in toluene T=110°C; 0.75 - 1.15 h; 2: octanoic acid chloride in toluene T=45 - 60°C; 1 - 2 h; 3: With water in toluene T=45°C; Product distribution / selectivity;
参考文献
US6777569 B1, ;
Page column 7-9 ;
反应条件
1: TESPT With sodium in Solventreg; 140 T=110°C; 0.75 h; 2: octanoic acid chloride in Solventreg; 140 T=45 - 104°C; 1 h; 3: With water in toluene T=45°C; Product distribution / selectivity;
参考文献
US6777569 B1, ;
Page column 9 ;
