反应条件
1: propargyl bromide With n-butyllithium; 1,1,1,3,3,3-hexamethyl-disilazane in tetrahydrofuran; hexane T=-78°C; 1 h; Inert atmosphere; 2: triethylsilyl chloride in tetrahydrofuran; hexane T=-78 - 20°C; 2.5 h; Inert atmosphere;
参考文献
Watanabe, Tsubasa; Imaizumi, Takamichi; Chinen, Takumi; Nagumo, Yoko; Shibuya, Masatoshi; Usui, Takeo; Kanoh, Naoki; Iwabuchi, Yoshiharu
Organic Letters, 2010 , vol. 12, # 5 p. 1040 - 1043
