N,N-二异丙基氨基硼烷合成路线 （共 54 条）
反应条件
triethylamine; bis-triphenylphosphine-palladium(II) chloride in 1,4-dioxane
T=70°C; 15 h;
参考文献
Euzenat, Lisenn; Horhant, David; Ribourdouille, Yann; Duriez, Christophe; Alcaraz, Gilles; Vaultier, Michel
Chemical Communications, 2003 , # 18 p. 2280 - 2281
反应条件
triethylamine; palladium in 1,4-dioxane
T=78°C; 15 h;
参考文献
Alcaraz, Gilles; Euzenat, Lisenn; Mongin, Olivier; Katan, Claudine; Ledoux, Isabelle; Zyss, Joseph; Blanchard-Desce, Mireille; Vaultier, Michel
Chemical Communications, 2003 , # 22 p. 2766 - 2767
反应条件
p-BrC6H4N(CH3)2, or p-IC6H4N(CH3)2; triethylamine; palladium in 1,4-dioxane
2 equiv. of B compd., 5 equiv. of amine, 15 h at 78°C;
参考文献
Alcaraz, Gilles; Euzenat, Lisenn; Mongin, Olivier; Katan, Claudine; Ledoux, Isabelle; Zyss, Joseph; Blanchard-Desce, Mireille; Vaultier, Michel
Chemical Communications, 2003 , # 22 p. 2766 - 2767
反应条件
1: tBuCH2CH2B(H)NiPr2; 3-bromobenzenediazonium tetrafluoroborate With biscyclopentadienyliron(II) in acetonitrile
T=20°C; 2.5 h;
2: With methanol in acetonitrile
T=0 - 20°C; 1 h;
3: 2,3-dimethylbutane-2,3-diol in diethyl ether; acetonitrile
T=20°C; 4 h; Reagent/catalyst;
参考文献
UNIVERSITE DE BORDEAUX 1; CENTRE NATIONAL DE LA RECHERCHE SCIENTIFIQUE; PUCHEAULT, Mathieu Jonathan Damien; MARCIASINI, Ludovic Daniel Alain; VAULTIER, Michel
Patent: WO2014/9169 A1, 2014 ;
Location in patent: Page/Page column 63-64 ;
