4-(3-甲酰基苯基)苯甲酸甲酯合成路线 (共 4 条)
反应条件
in N,N-dimethyl-formamide T=20°C; 2 h;
参考文献
WO2008/28118 A1, ;
Page/Page column 65-66 ;
反应条件
sodium methylate; lithium chloride; Palladacycle 1.) NMP, 90 deg C; 2.) THF, MeOH, reflux, 12 h; Yield givenMultistep reaction;
参考文献
Tetrahedron Letters, , vol. 40, # 3 p. 415 - 418
反应条件
sodium borohydride; acetic acid in ethanol
参考文献
Smith, Jessica M.; Vitali, Francesca; Archer, Steven A.; Fasan, Rudi
Angewandte Chemie - International Edition, 2011 , vol. 50, # 22 p. 5075 - 5080
反应条件
1: sodium tetrahydroborate / ethanol / 20 °C / Cooling with ice 2: phosphorus tribromide / dichloromethane / 20 °C / Inert atmosphere; Cooling with ice View Scheme
参考文献
Smith, Jessica M.; Vitali, Francesca; Archer, Steven A.; Fasan, Rudi
Angewandte Chemie - International Edition, 2011 , vol. 50, # 22 p. 5075 - 5080