2-(苯甲酰基)苯甲酰氯合成路线 （共 26 条）
反应条件
1: 2-benzoylbenzoyl chloride With 1-methyl-pyrrolidin-2-one in toluene T=0°C; 0.5 h; 2: phenyl-magnesium bromide in tetrahydrofuran; toluene T=-10 - 0°C; 4.25 h; chemoselective reaction;
参考文献
Gowda, Maravanhalli Sidde; Pande, Sushanth Sudhir; Ramakrishna, Ramesha Andagar; Prabhu, Kandikere Ramaiah
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 15 p. 5365 - 5368
反应条件
1: tetrahydrofuran / 1 h / 0 °C 2: 96 percent / NaBH4 / methanol / 1 h / Ambient temperature 3: conc. aq. HCl / CHCl3 / 1 h / Ambient temperature View Scheme
参考文献
Katsura, Yousuke; Zhang, Xiaoyan; Homma, Koichi; Rice, Kenner C.; Calderon, Silvia N.; Rothman, Richard B.; Yamamura, Henry I.; Davis, Peg; Flippen-Anderson, Judith L.; Xu, Heng; Becketts, Karen; Foltz, Eric J.; Porreca, Frank
Journal of Medicinal Chemistry, 1997 , vol. 40, # 18 p. 2936 - 2947
反应条件
triethylamine in chloroform Ambient temperatureovernight; Yield given;
参考文献
Shklyaev, V. S.; Veikhman, G. A.; Chupina, Yu. M.; Potemkin, K. D.
J. Gen. Chem. USSR (Engl. Transl.), 1984 , vol. 54, # 4 p. 919 - 925,819 - 824
反应条件
ammonium hydroxide
T=0°C;
参考文献
Graebe; Ullmann
Justus Liebigs Annalen der Chemie, 1896 , vol. 291, p. 16
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Haller; Guyot
Bulletin de la Societe Chimique de France, 1901 , vol. <3> 25, p. 53
参考文献
Hubacher
Journal of the American Chemical Society, 1943 , vol. 65, p. 1655
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Blicke; Swisher
Journal of the American Chemical Society, 1934 , vol. 56, p. 923
Journal of the American Chemical Society, 1935 , vol. 57, p. 2737
反应条件
pyridine in chloroform
Heating;
参考文献
Blicke; Swisher
Journal of the American Chemical Society, 1934 , vol. 56, p. 923
Journal of the American Chemical Society, 1935 , vol. 57, p. 2737
参考文献
Blicke; Swisher
Journal of the American Chemical Society, 1934 , vol. 56, p. 923
Journal of the American Chemical Society, 1935 , vol. 57, p. 2737
反应条件
Reaktion von Kalium-phenolat;
参考文献
Blicke; Swisher
Journal of the American Chemical Society, 1934 , vol. 56, p. 923
Journal of the American Chemical Society, 1935 , vol. 57, p. 2737
反应条件
aluminium trichloride
参考文献
Haller; Guyot
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1894 , vol. 119, p. 140
Bulletin de la Societe Chimique de France, 1901 , vol. <3> 25, p. 51
Full Text Show Details
Meyer,H.
Monatshefte fuer Chemie, 1904 , vol. 25, p. 1199
Chemische Berichte, 1905 , vol. 38, p. 2490
参考文献
Egerer; Meyer,H.
Monatshefte fuer Chemie, 1913 , vol. 34, p. 69
