1-(4-吡咯-1-苯基)-乙酮合成路线 (共 11 条)
反应条件
ionic liquid immobilized on γ-Fe2O3(at)SiO2 nanoparticles in water T=100°C; Clauson-Kaas Synthesis; 0.833333 h;
参考文献
More, Uttam A.; Joshi, Shrinivas D.; Aminabhavi, Tejraj M.; Gadad, Andanappa K.; Nadagouda, Mallikarjuna N.; Kulkarni, Venkatrao H.
European Journal of Medicinal Chemistry, 2014 , vol. 71, p. 199 - 218
反应条件
copper (II) acetate monohydrate; caesium carbonate in N,N-dimethyl-formamide T=110°C; 24 h; Inert atmosphere;
参考文献
Xu, Zhong-Lin; Li, Hong-Xi; Ren, Zhi-Gang; Du, Wei-Yuan; Xu, Wei-Chang; Lang, Jian-Ping
Tetrahedron, 2011 , vol. 67, # 29 p. 5282 - 5288
反应条件
copper(l) iodide; caesium carbonate; benzoyl-N'-phenylhydrazine in dimethyl sulfoxide T=120°C; Ullmann cross-coupling reaction; 24 h; Inert atmosphere;
参考文献
Li, Liuyi; Zhu, Lei; Chen, Dagui; Hu, Xuelei; Wang, Ruihu
European Journal of Organic Chemistry, 2011 , # 14 p. 2692 - 2696
反应条件
copper(I) oxide; copper; caesium carbonate in dimethyl sulfoxide T=150°C; 18 h;
参考文献
Son, Seung Uk; Park, In Kyu; Park, Jongnam; Hyeon, Taeghwan
Chemical Communications, 2004 , # 7 p. 778 - 779
反应条件
Grubb's 2nd generation catalyst; CuCl2·2H2O; oxygen in 1,2-dichloro-ethane T=60°C; 24 h;
参考文献
Chen, Weiqiang; Wang, Jianhui
Organometallics, 2013 , vol. 32, # 6 p. 1958 - 1963
反应条件
sodium tetrahydroborate; sulfuric acid; water in tetrahydrofuran; methanol T=10 - 20°C; 1.5 h; Yield given;
参考文献
Verardo, Giancarlo; Dolce, Anna; Toniutti, Nicoletta
Synthesis, 1999 , # 1 p. 74 - 79
反应条件
RuCl2(tricyclohexylphosphine)2(benzylidene); FeCl3·6H2O; oxygen in dichloromethane T=40°C; Grubbs Olefin Metathesis; 24 h;
参考文献
Organometallics, , vol. 32, # 6 p. 1958 - 1963
反应条件
tert.-butylhydroperoxide in water; benzene T=20°C; 0.5 h; Inert atmosphere;
参考文献
Schmidt, Bernd; Krehl, Stefan; Jablowski, Eric
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 26 p. 5119 - 5130
反应条件
potassium carbonate in N,N-dimethyl-formamide T=110°C; 18 h;
参考文献
European Journal of Medicinal Chemistry, , vol. 43, # 7 p. 1530 - 1535
反应条件
1: sodium carbonate / ethanol; water / 80 °C / Inert atmosphere 2: RuCl2(tricyclohexylphosphine)2(benzylidene) / benzene / 0.5 h / 20 °C / Inert atmosphere 3: tert.-butylhydroperoxide / water; benzene / 0.5 h / 20 °C / Inert atmosphere View Scheme
参考文献
Organic and Biomolecular Chemistry, , vol. 10, # 26 p. 5119 - 5130