3-甲氧基-4-硝基苯乙酮合成路线 （共 8 条）
反应条件
1: malonic acid dimethyl ester With triethylamine; magnesium chloride in toluene T=20°C; 1.5 h; 2: 4-nitro-3-methoxy-benzoylchloride in toluene 0.75 h; 3: With water in dimethyl sulfoxide Heating;
参考文献
Michaelides, Michael R.; Curtin, Michael L.; Dai, Yujia; Davidsen, Steven K.; Frey, Robin R.; Guo, Yan; Ji, Zhiqin
Patent: US2003/225273 A1, 2003 ;
Location in patent: Page 36 ;
反应条件
1.1: n-BuLi / tetrahydrofuran; hexane / 0.25 h 1.2: DDQ / tetrahydrofuran; hexane 2.1: H2SO4 / H2O; dioxane View Scheme
参考文献
Journal of Chemical Research - Part S, , # 8 p. 504 - 505
反应条件
1: KMnO4 / H2O / Heating 2: SOCl2 3: (i) Mg, (ii) H2SO4, AcOH View Scheme
参考文献
Bulletin de la Societe Chimique de France, , p. 2255 - 2261
参考文献
Magnetic Resonance in Chemistry, , vol. 30, # 6 p. 497 - 499
反应条件
1: SOCl2 2: (i) Mg, (ii) H2SO4, AcOH View Scheme
参考文献
Bulletin de la Societe Chimique de France, , p. 2255 - 2261
反应条件
(i) Mg, (ii) H2SO4, AcOH; Multistep reaction;
参考文献
Bulletin de la Societe Chimique de France, , p. 2255 - 2261
反应条件
bromine in acetic acid
参考文献
Julia,M.; Chastrette,F.
Bulletin de la Societe Chimique de France, 1962 , p. 2255 - 2261
反应条件
1: dimethylformamide / 0.67 h / 100 °C 2: cyclohexane / Pd/C / ethanol / 1 h / Heating View Scheme
参考文献
Tois, Jan; Vahermo, Mikko; Koskinen, Ari
Tetrahedron Letters, 2005 , vol. 46, # 5 p. 735 - 737
