N-(6-溴吡啶-2-基)三甲基乙酰胺合成路线 （共 4 条）
反应条件
triethylamine in toluene T=20 - 45°C; 25 h;
参考文献
Mase; Houpis; Akao; Dorziotis; Emerson; Hoang; Iida; Itoh; Kamei; Kato; Kawasaki; Lang; Lee; Lynch; Maligres; Molina; Nemoto; Okada; Reamer; Song; Tschaen; Wada; Zewge; Volante; Reider; Tomimoto
Journal of Organic Chemistry, 2001 , vol. 66, # 20 p. 6775 - 6786
反应条件
hydrogenchloride; triethylamine in toluene
参考文献
US2001/51727 A1, ;
US 20010051727 A1
反应条件
1: ammonia / H2O / 5 h / 190 °C 2: NEt3 / CH2Cl2 / 0 - 20 °C View Scheme
参考文献
Angewandte Chemie - International Edition, , vol. 44, # 11 p. 1640 - 1643
反应条件
1: 2-bromo-6-N-pivaloylaminopyridine With isopropylmagnesium chloride in tetrahydrofuran; toluene
T=5°C; 24 h;
2: N,N-dimethyl-formamide in tetrahydrofuran; toluene
T=10 - 15°C; 0.583333 h; Further stages.;
参考文献
Mase; Houpis; Akao; Dorziotis; Emerson; Hoang; Iida; Itoh; Kamei; Kato; Kawasaki; Lang; Lee; Lynch; Maligres; Molina; Nemoto; Okada; Reamer; Song; Tschaen; Wada; Zewge; Volante; Reider; Tomimoto
Journal of Organic Chemistry, 2001 , vol. 66, # 20 p. 6775 - 6786
